6-(对甲苯磺酰基)-2-噁-6-氮杂螺[3.3]庚烷合成路线 （共 5 条）
反应条件
potassium hydroxide in ethanol 90 h; Reflux;
参考文献
Chen, Xing-Xiu; Gao, Feng; Wang, Qi; Huang, Xing; Wang, Dan
Fitoterapia, 2014 , vol. 92, p. 111 - 115
反应条件
hydrogen bromide in diethyl ether; acetic acid T=0 - 20°C; 1.33333 h;
参考文献
UNIVERSITY HEALTH NETWORKS; Pauls, Heinz W.; Laufer, Radoslaw; Li, Sze-Wan; Ng, Grace
Patent: US2014/5167 A1, 2014 ;
Location in patent: Paragraph 0221; 0222 ;
反应条件
1: hydrogen bromide / diethyl ether; acetic acid / 1.33 h / 0 - 20 °C 2: carbon tetrabromide; triphenylphosphine / dichloromethane / 6 h / 0 - 20 °C View Scheme
参考文献
UNIVERSITY HEALTH NETWORKS; Pauls, Heinz W.; Laufer, Radoslaw; Li, Sze-Wan; Ng, Grace
Patent: US2014/5167 A1, 2014 ;
反应条件
1: magnesium / methanol / 1 h / |Sonication 2: ethanol; diethyl ether View Scheme
参考文献
Chen, Xing-Xiu; Gao, Feng; Wang, Qi; Huang, Xing; Wang, Dan
Fitoterapia, 2014 , vol. 92, p. 111 - 115
反应条件
methanol; magnesium 1 h; Sonication;
参考文献
Chen, Xing-Xiu; Gao, Feng; Wang, Qi; Huang, Xing; Wang, Dan
Fitoterapia, 2014 , vol. 92, p. 111 - 115
