1-CBZ-2-羟甲基吲哚啉合成路线 （共 3 条）
反应条件
sodium hydrogencarbonate in tetrahydrofuran; water
参考文献
Anderson, David John; Beauchamp, Thomas J.; Bundy, Gordon L.; Ciske, Fred L.; Farrell, John R.; Graber, David R.; Genin, Michael J.; Judge, Thomas M.; Moon, Malcolm Wilson; Schnute, Mark E.; Strohbach, Joseph Walter; Thaisrivongs, Suvit; Thorarensen, Atli; Turner, Steven Robert; Vaillancourt, Valerie A.; Wolf, Allison J.
Patent: US2002/25959 A1, 2002 ;
反应条件
1: thionyl chloride / 24 h / 20 °C / |Cooling with ice 2: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 20 °C 3: sodium tetrahydroborate; calcium chloride / tetrahydrofuran; methanol / 2 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 16, # 5 p. 1422 - 1425
反应条件
1: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 20 °C 2: sodium tetrahydroborate; calcium chloride / tetrahydrofuran; methanol / 2 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 16, # 5 p. 1422 - 1425
