苯并[b]噻吩-2-胺盐酸盐合成路线 (共 2 条)
反应条件
hydrogenchloride in 1,4-dioxane T=20°C;
参考文献
Branum, Shawn T.; Colburn, Raymond W.; Dax, Scott L.; Flores, Christopher M.; Jetter, Michele C.; Liu, Yi; Ludovici, Donald; Macielag, Mark J.; Matthews, Jay M.; McNally, James J.; Reaney, Laura M.; Russell, Ronald K.; Qin, Ning; Teleha, Christopher; Wells, Kenneth M.; Youells, Scott C.; Youngman, Mark A.
Patent: US2012/190674 A1, 2012 ;
Location in patent: Page/Page column 73 ;
反应条件
1: N-ethyl-N,N-diisopropylamine; diphenyl phosphoryl azide / 8 h / Reflux 2: hydrogenchloride / 1,4-dioxane / 20 °C View Scheme
参考文献
Branum, Shawn T.; Colburn, Raymond W.; Dax, Scott L.; Flores, Christopher M.; Jetter, Michele C.; Liu, Yi; Ludovici, Donald; Macielag, Mark J.; Matthews, Jay M.; McNally, James J.; Reaney, Laura M.; Russell, Ronald K.; Qin, Ning; Teleha, Christopher; Wells, Kenneth M.; Youells, Scott C.; Youngman, Mark A.
Patent: US2012/190674 A1, 2012 ;