(E)-4,5-二氧代十六碳-2-烯酸合成路线 （共 4 条）
反应条件
Candida antarctica lipase B in water T=20°C; 2 h;
参考文献
Eriksson, Johan; Johansson, Martin; Sterner, Olov
Tetrahedron Letters, 2002 , vol. 43, # 5 p. 891 - 893
反应条件
1: LDA / tetrahydrofuran / -78 - 20 °C 2: 51 percent / K3Fe(CN)6; OsO4; K2CO3 / quinuclidine; methaneslfone amide / 2-methyl-propan-2-ol; H2O / 96 h 3: 100 percent / TEMPO / CH2Cl2 / 0 °C 4: 70 percent / Candida antarctica Lipase B / various solvent(s); H2O / 2 h / 20 °C View Scheme
参考文献
Eriksson, Johan; Johansson, Martin; Sterner, Olov
Tetrahedron Letters, 2002 , vol. 43, # 5 p. 891 - 893
反应条件
1: 51 percent / K3Fe(CN)6; OsO4; K2CO3 / quinuclidine; methaneslfone amide / 2-methyl-propan-2-ol; H2O / 96 h 2: 100 percent / TEMPO / CH2Cl2 / 0 °C 3: 70 percent / Candida antarctica Lipase B / various solvent(s); H2O / 2 h / 20 °C View Scheme
参考文献
Eriksson, Johan; Johansson, Martin; Sterner, Olov
Tetrahedron Letters, 2002 , vol. 43, # 5 p. 891 - 893
反应条件
1: 100 percent / TEMPO / CH2Cl2 / 0 °C 2: 70 percent / Candida antarctica Lipase B / various solvent(s); H2O / 2 h / 20 °C View Scheme
参考文献
Eriksson, Johan; Johansson, Martin; Sterner, Olov
Tetrahedron Letters, 2002 , vol. 43, # 5 p. 891 - 893
