1-Boc-吡咯-2-硼酸合成路线 (共 13 条)
反应条件
in dimethyl sulfoxide; toluene Dean-StarkRefluxInert atmosphereSealed tubeSchlenk technique;
参考文献
Xu, Liang; Ding, Siyi; Li, Pengfei
Angewandte Chemie - International Edition, 2014 , vol. 53, # 7 p. 1822 - 1826
Angew. Chem., 2014 , vol. 126, # 7 p. 1853 - 1857,5
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethylene glycol dimethyl ether; water
T=20 - 60°C; 2 h; Inert atmosphere;
参考文献
Maeda, Hiromitsu; Kinoshita, Kota; Naritani, Kazumasa; Bando, Yuya
Chemical Communications, 2011 , vol. 47, # 29 p. 8241 - 8243
反应条件
palladium diacetate; sodium carbonate; tris-(o-tolyl)phosphine in water; N,N-dimethyl-formamide
Suzuki coupling;
参考文献
Hughes, Terry V.; Emanuel, Stuart L.; O'Grady, Harold R.; Connolly, Peter J.; Rugg, Catherine; Fuentes-Pesquera, Angel R.; Karnachi, Prabha; Alexander, Richard; Middleton, Steven A.
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 18 p. 5130 - 5133