antimony(V) pentachloride; SbF3 T=125 - 130°C; 24 h;

1: 77.5 percent / AlCl3 / 1.) 75 deg C, 1.5 h, 2.) 85 deg C, 1 h, 3.) 95 deg C, 1 h, 4.) 115 deg C, 24 h 2: 68 percent / activated zinc dust / diethyl ether / 3 h / Heating 3: 79 percent / Cl2 / 96 h / 110 °C 4: 82 percent / SbF3, SbCl5 / 24 h / 125 - 130 °C View Scheme

1: 68 percent / activated zinc dust / diethyl ether / 3 h / Heating 2: 79 percent / Cl2 / 96 h / 110 °C 3: 82 percent / SbF3, SbCl5 / 24 h / 125 - 130 °C View Scheme

1: 79 percent / Cl2 / 96 h / 110 °C 2: 82 percent / SbF3, SbCl5 / 24 h / 125 - 130 °C View Scheme