aluminium trichloride; BTPPD in acetonitrile 0.025 h; microwave irradiation;

1: With bis(acetylacetonate)oxovanadium; (R)-2-((1-hydroxy-3,3-dimethylbutan-2-ylimino)methyl)-4,6-diiodophenol in chloroform T=20°C; 0.5 h; 2: With dihydrogen peroxide in chloroform T=0°C;

1: With RhCl(PPh3)3 in tetrahydrofuran T=25°C; 4 h; 2: With sodium hydroxide; dihydrogen peroxide in tetrahydrofuran Title compound not separated from byproducts;

1: With N-benzyl-N,N,N-trimethyl-ammonium chloride; triphenylphosphine; bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate in tetrahydrofuran T=25°C; 4 h; 2: With sodium hydroxide; dihydrogen peroxide in tetrahydrofuran Title compound not separated from byproducts;

1: natrium carbonate View Scheme

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T=140°C;

暂无反应条件数据