苯甲酮-2,4,5-三羧酸合成路线 （共 7 条）
反应条件
1: With nitric acid in water 120 h; Heating; 2: With sodium hydroxide; potassium permanganate in water
参考文献
Lohier, Jean-Francois; Wright, Karen; Peggion, Cristina; Formaggio, Fernando; Toniolo, Claudio; Wakselman, Michel; Mazaleyrat, Jean-Paul
Tetrahedron, 2006 , vol. 62, # 26 p. 6203 - 6213
反应条件
1.1: 67 percent / AlCl3 / CH2Cl2 2.1: HNO3 / H2O / 120 h / Heating 2.2: 61 percent / NaOH; KMnO4 / H2O View Scheme
参考文献
Tetrahedron, , vol. 62, # 26 p. 6203 - 6213
反应条件
1: 73 percent / AlCl3 / CH2Cl2 / 6 h / Ambient temperature 2: 1) 20percent HNO3, 2) KMnO4, 10percent aq.NaOH / 1) reflux, 5 d, 2) reflux, 3 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 56, # 21 p. 6243 - 6245
反应条件
1: With aluminium trichloride 16 h; Heating; 2: With water 0.5 h;
参考文献
Russian Journal of General Chemistry, , vol. 75, # 7 p. 1151 - 1156
反应条件
T=200°C; im Druckrohr;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 35, p. 503
反应条件
sulfuric acid T=120 - 130°C; 3 h;
参考文献
Lohier, Jean-Francois; Wright, Karen; Peggion, Cristina; Formaggio, Fernando; Toniolo, Claudio; Wakselman, Michel; Mazaleyrat, Jean-Paul
Tetrahedron, 2006 , vol. 62, # 26 p. 6203 - 6213
反应条件
1: sulfuric acid monohydrate / 5 h / 150 °C
2: 50 percent / oleum / 6 h / Heating
View Scheme
参考文献
Borisov; Maizlish; Shaposhnikov
Russian Journal of General Chemistry, 2005 , vol. 75, # 7 p. 1151 - 1156
