sodium carbonate; (S)-4,4-Br2-4,5-dihydro-3H-dinaphtho[2,1-c:1',2'-e]stannepin in tetrahydrofuran; water T=-10°C; 17 h; Title compound not separated from byproducts.;
lithium aluminium tetrahydride in tetrahydrofuran
T=20°C; 2 h; Inert atmosphere;
参考文献
Baez-Santos, Yahira M.; Barraza, Scott J.; Wilson, Michael W.; Agius, Michael P.; Mielech, Anna M.; Davis, Nicole M.; Baker, Susan C.; Larsen, Scott D.; Mesecar, Andrew D.
Journal of Medicinal Chemistry, 2014 , vol. 57, # 6 p. 2393 - 2412