反应条件
1: 4.78 g / potassium carbonate / methanol / 1 h / 20 °C
2: 74 percent / N-methylmorpholine N-oxide; tetra-n-propylammonium perruthenate; 4 Angstroem molecular sieves / acetonitrile / 1.5 h / 20 °C
3: Amberlyst 15 / acetone / 48 h / 20 °C
4: 0.19 g / Amberlyst 15 / acetone / 48 h / 20 °C
5: tetrabutylammonium fluoride / tetrahydrofuran / 96 h / 20 °C
6: 810 mg / NaHCO3; Dess-Martin periodinane / CH2Cl2 / 1.5 h / 20 °C
7: triethylamine / dimethylformamide / 43 h / 130 °C
8: 567 mg / dimethyldioxirane / CH2Cl2 / -78 - 20 °C
9: 90 percent / triethylamine / dimethylformamide / 48 h / 125 °C
10: 94 percent / phenylselenium bromide / CH2Cl2 / 2 h / 0 - 10 °C
11: 86 percent / sodium borohydride / methanol / 1 h / 0 °C
12: 19 mg / toluene / 4 h / 80 °C
13: 98 percent / tetrabutylammoonium fluoride / tetrahydrofuran / 3 h / 20 °C
14: 68 percent / polymer supported para-toluenesulfonic acid; 4 Angstroem molecular sieves / CH2Cl2 / 16 h / 20 °C
15: aq. HCl / methanol / 2 h / 40 °C
16: 3 mg / 4-N,N-dimethylaminopyridine / CH2Cl2 / 1 h / 20 °C
View Scheme
参考文献
Andrews, Stephen P.; Ball, Matthew; Wierschem, Frank; Cleator, Ed; Oliver, Steven; Hoegenauer, Klemens; Simic, Oliver; Antonello, Alessandra; Huenger, Udo; Smith, Martin D.; Ley, Steven V.
Chemistry - A European Journal, 2007 , vol. 13, # 20 p. 5688 - 5712
