反应条件
1: diethylzinc; (Z)-1-Iodo-non-4-ene With copper(l) iodide
T=60°C; 16 h;
2: 1-tetrahydropyranyloxy-9-iodo-2-nonyne With N,N'-dimethyl-N,N'-propyleneurea; Me2Cu(CN)(MgCl)2 in tetrahydrofuran
T=-78 - 0°C; Further stages. Title compound not separated from byproducts.;
参考文献
Capdevila, Anna; Prasad, Attaluri R.; Quero, Carmen; Petschen, Ines; Bosch, Maria P.; Guerrero, Angel
Organic Letters, 1999 , vol. 1, # 6 p. 845 - 848