1-环丙基-3-苯基-1-丙酮合成路线 (共 5 条)
反应条件
manganese; chloro-trimethyl-silane; PbCl2; 4-(N,N-dimethlyamino)pyridine in tetrahydrofuran; N,N-dimethyl-formamide T=25°C; 0.3 h;
参考文献
Takai, Kazuhiko; Ueda, Takashi; Ikeda, Norihiko; Ishiyama, Takaya; Matsushita, Hiroshi
Bulletin of the Chemical Society of Japan, 2003 , vol. 76, # 2 p. 347 - 353
反应条件
copper(l) iodide in tetrahydrofuran T=-78 - 20°C; 18 h;
参考文献
Chan, Louis K. M.; Poole, Darren L.; Shen, Di; Healy, Mark P.; Donohoe, Timothy J.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 3 p. 761 - 765
Angew. Chem., 2014 , vol. 126, # 3 p. 908
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; triphenylphosphine; potassium hydroxide T=100°C; 4 h; Inert atmosphereSealed tube;
参考文献
Chan, Louis K. M.; Poole, Darren L.; Shen, Di; Healy, Mark P.; Donohoe, Timothy J.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 3 p. 761 - 765
Angew. Chem., 2014 , vol. 126, # 3 p. 908
反应条件
nickel P=14710.2 Torr; Hydrogenation;
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 241, p. 602
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 241, p. 602