2-乙酰基-6-硝基苯甲酸合成路线 （共 12 条）
反应条件
L-Val hydrochloride in water; toluene T=90°C; 6 h;
参考文献
Luethy, Christoph; Zondler, Helmut; Rapold, Thomas; Seifert, Gottfried; Urwyler, Bernhard; Heinis, Thomas; Steinruecken, Hans Christian; Allen, James
Pest Management Science, 2001 , vol. 57, # 3 p. 205 - 224
反应条件
hydrogenchloride in water T=90°C; Decarboxylation; hydrolysis;
参考文献
Tamaru, Masatoshi; Saito, Yoshihiro
Pesticide Science, 1996 , vol. 47, # 2 p. 125 - 130
参考文献
Baker et al.
Journal of Organic Chemistry, 1952 , vol. 17, p. 149,153
Full Text Show Details
Horii et al.
Yakugaku Zasshi, 1954 , vol. 74, p. 471,473
Chem.Abstr., 1955 , p. 6883
参考文献
Horii et al.
Yakugaku Zasshi, 1954 , vol. 74, p. 471,473
Chem.Abstr., 1955 , p. 6883
反应条件
hydrogen; palladium on activated charcoal; 5 percent palladium-carbon in 1,4-dioxane T=30 - 100°C; P=1500.12 Torr; 41 h;
参考文献
Luethy, Christoph; Zondler, Helmut; Rapold, Thomas; Seifert, Gottfried; Urwyler, Bernhard; Heinis, Thomas; Steinruecken, Hans Christian; Allen, James
Pest Management Science, 2001 , vol. 57, # 3 p. 205 - 224
反应条件
hydrogen; palladium 10 on activated carbon in water T=80°C; P=2925.29 Torr; pH=12; 1 h; Product distribution / selectivity;
参考文献
EP2316818 A1, ;
Page/Page column 6-7 ;
反应条件
1: hydrogen / palladium 10 on activated carbon / water / 1 h / 80 °C / 2925.29 Torr / pH 1 2: hydrogen / palladium 10 on activated carbon / water / 1 h / 80 °C / 2925.29 Torr / pH 12 View Scheme
参考文献
Active Biotech AB
Patent: EP2316818 A1, 2011 ;
反应条件
hydrogen; palladium on activated charcoal; 5 percent palladium-carbon in 1,4-dioxane T=30 - 100°C; P=1500.12 Torr; 41 h;
参考文献
Luethy, Christoph; Zondler, Helmut; Rapold, Thomas; Seifert, Gottfried; Urwyler, Bernhard; Heinis, Thomas; Steinruecken, Hans Christian; Allen, James
Pest Management Science, 2001 , vol. 57, # 3 p. 205 - 224
反应条件
hydrogen; platinum(IV) oxide in water T=80°C; P=2925.29 Torr; pH=12; 1 h; Product distribution / selectivity;
参考文献
ACTIVE BIOTECH AB; JANSSON, Karl
Patent: WO2011/54874 A1, 2011 ;
Location in patent: Page/Page column 10 ;
反应条件
hydrogen; palladium 10 on activated carbon in water T=80°C; P=2925.29 Torr; pH=12; 1 h; Product distribution / selectivity;
参考文献
ACTIVE BIOTECH AB; JANSSON, Karl
Patent: WO2011/54874 A1, 2011 ;
Location in patent: Page/Page column 10 ;
