2-乙酰基-6-硝基苯甲酸合成路线 （共 12 条）
反应条件
1: 93.2 percent / H2; NaOH / 5 percent Pd/C / H2O / 30 - 35 °C / 1500.12 Torr 2: 80.9 percent / NaBH4; NaOH / H2O / 1 h / pH 11 / Heating View Scheme
参考文献
Active Biotech AB
Patent: EP2316818 A1, 2011 ;
反应条件
1.1: H2 / 5 percent Pd/C / dioxane / 41 h / 30 - 100 °C / 1500.12 Torr
2.1: 37 percent HCl; NaNO2 / H2O / -5 - 0 °C
2.2: potassium xanthogenate; sodium hydroxide / H2O / 0.67 h / 30 - 40 °C
3.1: 90.4 percent / K2CO3 / dimethylformamide / 2.5 h / 50 °C
View Scheme
参考文献
Luethy, Christoph; Zondler, Helmut; Rapold, Thomas; Seifert, Gottfried; Urwyler, Bernhard; Heinis, Thomas; Steinruecken, Hans Christian; Allen, James
Pest Management Science, 2001 , vol. 57, # 3 p. 205 - 224
