5,7-二甲基-1-萘满酮合成路线 （共 25 条）
反应条件
acetone in toluene T=80°C; 0.3 h; Flow reactor;
参考文献
Chorghade, Rajeev; Battilocchio, Claudio; Hawkins, Joel M.; Ley, Steven V.
Organic Letters, 2013 , vol. 15, # 22 p. 5698 - 5701
参考文献
Greenland, Harry; Kozyrod, Robert P.; Pinhey, John T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 2011 - 2016
反应条件
aluminium trichloride T=75°C; 20 h;
参考文献
Jung; Koreeda
Journal of Organic Chemistry, 1989 , vol. 54, # 24 p. 5667 - 5675
反应条件
in benzene T=295 - 340°C;
参考文献
Journal of Organic Chemistry, , vol. 47, # 26 p. 5096 - 5099
反应条件
bis(acetylacetonate)nickel(II); air; trimethylaluminum; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; phenol 1.) hexane, THF, room temperature, 2 h, 2.) overnight; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 119, # 20 p. 4779 - 4780
反应条件
phosphoric acid T=160°C;
参考文献
Journal of the Chemical Society, , p. 798
反应条件
1: palladium; acetic acid / 50 °C / 2206.5 Torr / Hydrogenation 2: polyphosphoric acid View Scheme
参考文献
Journal of Organic Chemistry, , vol. 18, p. 485,488
反应条件
(i) AlCl3, (ii) polyphosphoric acid; Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 36, # 17 p. 2480 - 2485
反应条件
aluminium trichloride; Petroleum ether
参考文献
Journal of the Chemical Society, , p. 2537,2540
参考文献
Journal of the Chemical Society, , p. 232,235
