反应条件
1.1: NaBH4 / methanol / 20 °C
2.1: 83.3 percent / 4-toluenesulfonic acid / toluene / 5 h / Heating
3.1: NaOCl; 4-phenylpyridine N-oxide; (R,R)-Jaconsen's catalyst / CH2Cl2 / 0 °C
4.1: MeCN; TfOH / 1 h / 20 °C
4.2: H2O / 5 h / Heating
View Scheme
参考文献
Marino, Sharon T.; Stachurska-Buczek, Danuta; Huggins, Daniel A.; Krywult, Beata M.; Sheehan, Craig S.; Nguyen, Thao; Choi, Neil; Parsons, Jack G.; Griffiths, Peter G.; James, Ian W.; Bray, Andrew M.; White, Jonathan M.; Boyce, Rustum S.
Molecules, 2004 , vol. 9, # 6 p. 405 - 426
