4-(4-戊基环己基)苯硼酸合成路线 （共 3 条）
反应条件
1: With n-butyllithium in tetrahydrofuran T=-78°C; 0.5 h; 2: With tri-isopropoxy-borane in tetrahydrofuran T=-78 - 20°C;
参考文献
Lee, Jong-Beom; Lee, Hyun-Kyung; Park, Jae-Chul; Kim, Yong-Bae
Molecular Crystals and Liquid Crystals, 2005 , vol. 439, p. 161/[2027]-172/[2038]
反应条件
1.1: 91 percent / iron; bromine / CHCl3 / 12 h 2.1: nBuLi / tetrahydrofuran / 0.5 h / -78 °C 2.2: 71 percent / triisopropyl borate / tetrahydrofuran / -78 - 20 °C View Scheme
参考文献
Lee, Jong-Beom; Lee, Hyun-Kyung; Park, Jae-Chul; Kim, Yong-Bae
Molecular Crystals and Liquid Crystals, 2005 , vol. 439, p. 161/[2027]-172/[2038]
反应条件
1: para-(trans-4-n-pentylcyclohexyl)bromobenzene With magnesium in tetrahydrofuran 2: boric acid trimethyl ester in tetrahydrofuran
参考文献
Matsushita, Satoshi; Yan, Bairu; Yamamoto, Shinsuke; Jeong, Yong Soo; Akagi, Kazuo
Angewandte Chemie - International Edition, 2014 , vol. 53, # 6 p. 1659 - 1663
Angew. Chem., 2014 , vol. 126, # 6 p. 1685 - 1689,5
