反应条件
in diethyl ether
addn. of Ph(CH2)4HgBr in ether to mixt. of Ph(CH2)4Br and Mg in ether, boiling (stirring, 4 h); addn. of water and aq. NH4Cl, sepn. of org. layer, extn. of aq. phase (ether), drying (over Na2SO4), removal of solvent (vac.), distn. 130-150°C, 8E-4 mm); mass spectroscopy;
参考文献
Kaganovich, V. S.; Rybinskaya, M. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1471 - 1475
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , vol. 33, p. 1601 - 1606
