3-丁烯-1-炔-1-基苯合成路线 （共 40 条）
反应条件
unter Druck.Hydrogenation;
参考文献
Golse
Annales de Chimie (Cachan, France), 1948 , vol. <12> 3, p. 527,554
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Quelet; Golse
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1947 , vol. 224, p. 661,662
Bulletin de la Societe Chimique de France, 1947 , p. 313,315
反应条件
(i) Li, Et2O, (ii) /BRN= 2037964/; Multistep reaction;
参考文献
Cherkasov,L.N. et al.
Zhurnal Organicheskoi Khimii, 1966 , vol. 2, p. 1938 - 1942,1906 - 1909
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); diethylamine in tetrahydrofuran
T=0 - 20°C; Inert atmosphere;
参考文献
Puenner, Florian; Hilt, Gerhard
Chemical Communications, 2012 , vol. 48, # 30 p. 3617 - 3619
反应条件
T=700°C; P=0.005 Torr; Flash vacuum pyrolysis;
参考文献
Padwa,A.; Caruso,T.; Nahm,S.
Journal of the American Chemical Society, 1982 , vol. 104, p. 2865
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=250°C;
参考文献
Collins, Clair J.; Hanack, Michael; Stutz, Herbert; Auchter, Gerhard; Schoberth, Winfried
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5260 - 5268
反应条件
hydrogenchloride in tetrahydrofuran
1 h; Ambient temperature;
参考文献
Shirakawa, Eiji; Yoshida, Hiroto; Kurahashi, Takuya; Nakao, Yoshiaki; Hiyama, Tamejiro
Journal of the American Chemical Society, 1998 , vol. 120, # 12 p. 2975 - 2976
反应条件
tris(dibenzylideneacetone)dipalladium (0); tris(4-methoxyphenyl)-phosphine; N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide
T=80°C; Stille reaction; 10 h;
参考文献
Shen, Wang; Wang, Le
Journal of Organic Chemistry, 1999 , vol. 64, # 24 p. 8873 - 8879
反应条件
tetrabutyl ammonium fluoride; copper diacetate in 1,4-dioxane
T=30°C;
参考文献
Arsenyan, Pavel; Petrenko, Alla; Paegle, Edgars; Belyakov, Sergey
Mendeleev Communications, 2011 , vol. 21, # 6 p. 326 - 328
反应条件
(4-CF3-Ph)3PAuCl; silver trifluoromethanesulfonate in dichloromethane
3 h; Reflux;
参考文献
Dombray, Thomas; Blanc, Aurelien; Weibel, Jean-Marc; Pale, Patrick
Organic Letters, 2010 , vol. 12, # 23 p. 5362 - 5365
反应条件
1: 96 percent / sodium hydride / dimethylformamide / 2 h / 25 °C
2: 88 percent / sodium hydride / dimethylformamide / 3 h
3: 700 °C / 0.01 Torr
View Scheme
参考文献
Padwa,A.; Caruso,T.; Nahm,S.
Journal of the American Chemical Society, 1982 , vol. 104, p. 2865
