3,3-双甲基磺酰基-1-苯丙酮合成路线 （共 47 条）
反应条件
1: 82 percent / n-BuLi / tetrahydrofuran / Heating
2: 81 percent / POCl3 / 0 - 90 °C
View Scheme
参考文献
Mahata; Venkatesh; Syam Kumar; Ila; Junjappa
Journal of Organic Chemistry, 2003 , vol. 68, # 10 p. 3966 - 3975
反应条件
1: 92 percent / tetrahydrofuran / 1 h, -70 deg C, than 1 h, r.t.
2: 91 percent / HCl / methanol; H2O / 1 h / Ambient temperature
3: 93 percent / BuLi / tetrahydrofuran / -10 °C
4: 54 percent / Raney Ni / ethanol / 0.5 h / Ambient temperature
View Scheme
参考文献
Okazaki, Renji; Negishi, Yoshio; Inamoto, Naoki
Journal of Organic Chemistry, 1984 , vol. 49, # 20 p. 3819 - 3824
反应条件
1: ethanol / 3 h / Heating
2: Lawesson's reagent / benzene / 0.5 h / Heating
View Scheme
参考文献
Lee, Dong Joon; Kim, Kyongtae
Journal of Organic Chemistry, 2004 , vol. 69, # 14 p. 4867 - 4869
反应条件
in xylene
24 h; Heating;
参考文献
Huang; Wang
Synthesis, 1992 , # 12 p. 1273 - 1276
反应条件
in 1,4-dioxane
Heating;
参考文献
Huang, Zhi-Tang; Wang, Mei-Xiang
Tetrahedron, 1992 , vol. 48, # 12 p. 2325 - 2332
参考文献
Kumar,A. et al.
Journal of the Chemical Society, Chemical Communications, 1976 , p. 593 - 594
反应条件
in methanol
Heating;
参考文献
Chauhan,S.M.S.; Junjappa,H.
Tetrahedron, 1976 , vol. 32, p. 1779 - 1787
