反-1,2-二(2-噻吩基)乙烯合成路线 （共 16 条）
反应条件
1: 46 percent / 1.) reflux, 10 h, 2.) 15 deg C, 12 h 2: 1.) NaH / 1.) DME, 15 deg C, 2.) reflux, 3 h View Scheme
参考文献
Synthesis, , # 8 p. 620 - 623
反应条件
sodium hydride 1.) DME, 15 deg C, 2.) reflux, 3 h; Yield given. Multistep reaction;
参考文献
Synthesis, , # 8 p. 620 - 623
反应条件
sodium hydride 1.) DME, 0 deg C, 0.5 h, 2.) DME, reflux, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Heterocycles, , vol. 32, # 5 p. 991 - 1002
反应条件
1: 1.) POCl3 / 1.) 0 deg C, 1 h, 2.) DMF, 50 deg C, 3 h 2: 1.) NaH / 1.) DME, 0 deg C, 30 min, 2.) DME, reflux, 3.5 h View Scheme
参考文献
Nakayama, Juzo; Fujimori, Toru
Heterocycles, 1991 , vol. 32, # 5 p. 991 - 1002
反应条件
trichlorophosphate in 1,2-dichloro-ethane Vilsmeier reaction; 2 h; Heating;
参考文献
Raimundo, Jean-Manuel; Blanchard, Philippe; Gallego-Planas, Nuria; Mercier, Nicolas; Ledoux-Rak, Isabelle; Hierle, Rolland; Roncali, Jean
Journal of Organic Chemistry, 2002 , vol. 67, # 1 p. 205 - 218
反应条件
oxygen; 5,15,10,20-tetraphenylporphyrin in tetrachloromethane T=20°C; Irradiation;
参考文献
Tetrahedron Letters, , vol. 43, # 37 p. 6633 - 6636
