2-甲氧基-4-硝苄基乙醇合成路线 (共 10 条)
反应条件
calcium carbonate in 1,4-dioxane; water Heating / reflux;
参考文献
US2004/214798 A1, ;
Page 17 ;
反应条件
methanol; sodium tetrahydroborate 12 h;
参考文献
WO2014/39412 A1, ;
Paragraph 00316 ;
反应条件
diisobutylaluminium hydride in tetrahydrofuran T=0°C; 1 h;
参考文献
Bulletin of the Korean Chemical Society, , vol. 32, # 5 p. 1461 - 1462
反应条件
sodium hydroxide in tetrahydrofuran; methanol
参考文献
US2003/195201 A1, ;
US 20030195201 A1
反应条件
sodium carbonate; bis(dibenzylideneacetone)-palladium(0); dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine in 1,4-dioxane; water Suzuki-Miyaura cross-coupling; 24 h; Inert atmosphereReflux;
参考文献
Organic Letters, , vol. 14, # 5 p. 1278 - 1281
反应条件
sodium hydroxide in methanol Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 52, # 7 p. 818 - 829
反应条件
1: N-bromosuccinimide; 2,2'-dimethyl-2,2'-diazenediyldipropanenitrile / ethyl acetate / Heating 2: AcOH / 120 °C 3: NaOH / methanol / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 52, # 7 p. 818 - 829
反应条件
1: potassium carbonate / 4 h / Reflux 2: diisobutylaluminium hydride / tetrahydrofuran / 1 h / 0 °C View Scheme
参考文献
Bulletin of the Korean Chemical Society, , vol. 32, # 5 p. 1461 - 1462
反应条件
dipyridinium dichromate in dichloromethane T=40°C; 3 h;
参考文献
Bhusal, Ram Prasad; Yun Cho, Pyo; Kim, Soon-Ai; Park, Hyun; Kim, Hak Sung
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 5 p. 1461 - 1462
反应条件
hydrogen bromide; acetic acid
参考文献
Palmer, Brian D.; Thompson, Andrew M.; Booth, R. John; Dobrusin, Ellen M.; Kraker, Alan J.; Lee, Ho H.; Lunney, Elizabeth A.; Mitchell, Lorna H.; Ortwine, Daniel F.; Smaill, Jeff B.; Swan, Leesa M.; Denny, William A.
Journal of Medicinal Chemistry, 2006 , vol. 49, # 16 p. 4896 - 4911