1,1'-[(2E)-2-丁烯-1,4-二基]二苯合成路线 (共 22 条)
反应条件
magnesium in methanol
Ambient temperaturereacted until the Mg had dissolved; Yield given. Yields of byproduct given;
参考文献
Hutchins, Robert O.; Suchismita
Tetrahedron Letters, 1989 , vol. 30, # 1 p. 55 - 56
反应条件
magnesium in methanol
Ambient temperaturereacted until the Mg had dissolved; Yield given. Yields of byproduct given;
参考文献
Hutchins, Robert O.; Suchismita
Tetrahedron Letters, 1989 , vol. 30, # 1 p. 55 - 56
反应条件
Grubb's 2nd generation catalyst in dichloromethane
20 h; Refluxsolid phase reaction;
参考文献
Poeylaut-Palena, Andres A.; Mata, Ernesto G.
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 17 p. 3947 - 3956
反应条件
1-aza-bicyclo[2.2.2]octane
Yield given. Multistep reaction;
参考文献
Opitz, Guenter; Ehlis, Thomas; Rieth, Karlheinz
Chemische Berichte, 1990 , vol. 123, # 10 p. 1989 - 1998
反应条件
Grubb's 2nd generation catalyst in dichloromethane
20 h; Refluxsolid phase reaction;
参考文献
Poeylaut-Palena, Andres A.; Mata, Ernesto G.
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 17 p. 3947 - 3956
反应条件
sodium hydride; dimethyl sulfoxide
1.) 30 min, 2.) 30 min; Yield given. Multistep reaction;
参考文献
Boehm; Gleason; Pendrak; Sarau; Schmidt; Foley; Kingsbury
Journal of Medicinal Chemistry, 1993 , vol. 36, # 22 p. 3333 - 3340
反应条件
sodium amalgam; ethanol
α,δ-diphenyl-β-butylene;
参考文献
Straus
Justus Liebigs Annalen der Chemie, 1905 , vol. 342, p. 257
反应条件
diethyl ether; ethanol
liquid form;
参考文献
Schlenk; Bergmann
Justus Liebigs Annalen der Chemie, 1928 , vol. 463, p. 208
反应条件
1: CuCl2
2: diethyl ether
View Scheme
参考文献
Dombrowskii; Terent'ew
Zhurnal Obshchei Khimii, 1956 , vol. 26, p. 2776,2782; engl. Ausg. S. 3091, 3096
参考文献
Dombrowskii; Terent'ew
Zhurnal Obshchei Khimii, 1956 , vol. 26, p. 2776,2782; engl. Ausg. S. 3091, 3096