2,2-二溴-1-苯乙酮合成路线 (共 82 条)
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kowalski, Conrad J.; Reddy, Rajarathnam E.
Journal of Organic Chemistry, 1992 , vol. 57, # 28 p. 7194 - 7208
反应条件
indium in N,N-dimethyl-formamide 3 h; Ambient temperatureultrasonication;
参考文献
Araki, Shuki; Hirashita, Tsunehisa; Shimizu, Ken; Ikeda, Takahiro; Butsugan, Yasuo
Tetrahedron, 1996 , vol. 52, # 8 p. 2803 - 2816
反应条件
lithium perchlorate in N,N-dimethyl-formamide Reduction; 1.5 h; Electrolysis; Product distribution; Further Variations:initial concentration;
参考文献
Batanero, Belen; Pastor, Gustavo; Barba, Fructuoso
Acta Chemica Scandinavica, 1999 , vol. 53, # 10 p. 910 - 912
反应条件
potassium hydroxide racemic mandelic acid;
参考文献
Engler; Woehrle
Chemische Berichte, 1887 , vol. 20, p. 2202
参考文献
Aston et al.
Journal of the American Chemical Society, 1942 , vol. 64, p. 1413,1414
反应条件
1: α,α-dibromo-1-phenylethanone With dimethyl sulfoxide T=70 - 75°C; Inert atmosphere; 2: methanol T=25 - 30°C; Inert atmosphere;
参考文献
Raghunadh, Akula; Meruva, Suresh Babu; Kumar, Nuka Anil; Kumar, Gudla Santosh; Rao, L. Vaikunta; Syamkumar
Synthesis, 2012 , vol. 2012, # 2 p. 283 - 289
反应条件
sodium hydroxide; ethanol; hydroxylamine hydrochloride; phenylglyoxime T=50 - 60°C;
参考文献
Russanow
Chemische Berichte, 1891 , vol. 24, p. 3502
反应条件
potassium hydroxide racemic mandelic acid;
参考文献
Engler; Woehrle
Chemische Berichte, 1887 , vol. 20, p. 2202
参考文献
Aston et al.
Journal of the American Chemical Society, 1942 , vol. 64, p. 1413,1414
反应条件
potassium hydroxide racemic mandelic acid;
参考文献
Engler; Woehrle
Chemische Berichte, 1887 , vol. 20, p. 2202