2,2-二溴-1-苯乙酮合成路线 (共 82 条)
参考文献
Aston et al.
Journal of the American Chemical Society, 1942 , vol. 64, p. 1413,1414
反应条件
sodium methylate in methanol 1 h; Ambient temperature;
参考文献
Boeykens, Marc; De Kimpe, Norbert
Tetrahedron, 1994 , vol. 50, # 43 p. 12349 - 12360
反应条件
1: sodium acetate; diluted alcohol; hydroxylamine hydrochloride / 70 - 80 °C 2: concentrated sulfuric acid / 100 °C View Scheme
参考文献
Ponzio; Avogadro
Gazzetta Chimica Italiana, 1923 , vol. 53, p. 316
反应条件
water; [C5mim][BF4] T=125°C; P=2585.74 Torr; 0.0416667 h; microwave irradiation;
参考文献
Ranu, Brindaban C.; Chattopadhyay, Kalicharan; Jana, Ranjan
Tetrahedron, 2007 , vol. 63, # 1 p. 155 - 159
反应条件
potassium cyanide; water in acetone T=20°C; chemoselective reaction;
参考文献
Tatar, Jovana; Markovic, Rade; Stojanovic, Milovan; Baranac-Stojanovic, Marija
Tetrahedron Letters, 2010 , vol. 51, # 37 p. 4851 - 4855
反应条件
mercury dichloride; zinc in diethyl ether; ethyl acetate T=55 - 60°C; 0.5 h;
参考文献
Shchepin, V. V.; Gladkova, G. E.; Russkikh, N. Yu.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 6.1 p. 902 - 907
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 6 p. 1156 - 1162
反应条件
T=15°C; sofortiges Ansaeuern mit Essigsaeure;
参考文献
Ayres; Hauser
Journal of the American Chemical Society, 1943 , vol. 65, p. 1095
反应条件
indium in N,N-dimethyl-formamide 3 h; Ambient temperatureultrasonication;
参考文献
Araki, Shuki; Hirashita, Tsunehisa; Shimizu, Ken; Ikeda, Takahiro; Butsugan, Yasuo
Tetrahedron, 1996 , vol. 52, # 8 p. 2803 - 2816
反应条件
in water T=70°C; 4 h;
参考文献
Madhav; Narayana Murthy; Anil Kumar; Ramesh; Nageswar
Tetrahedron Letters, 2012 , vol. 53, # 30 p. 3835 - 3838
反应条件
tert.-butyl lithium; lithium hexamethyldisilazane Yield given. Multistep reaction;
参考文献
Kowalski, Conrad J.; Fields, Kevin W.
Journal of the American Chemical Society, 1982 , vol. 104, # 1 p. 321 - 323