2,2-二溴-1-苯乙酮合成路线 （共 82 条）
反应条件
1: α,α-dibromo-1-phenylethanone With dimethyl sulfoxide T=70 - 75°C; Inert atmosphere; 2: isopropyl alcohol T=25 - 30°C; Inert atmosphere;
参考文献
Raghunadh, Akula; Meruva, Suresh Babu; Kumar, Nuka Anil; Kumar, Gudla Santosh; Rao, L. Vaikunta; Syamkumar
Synthesis, 2012 , vol. 2012, # 2 p. 283 - 289
反应条件
potassium phosphate; sodium iodide in sulfolane T=20 - 35°C; Inert atmosphere;
参考文献
Shankar; More, Satish S.; Madhubabu; Vembu; Syam Kumar
Synlett, 2012 , vol. 23, # 7 p. 1013 - 1020
反应条件
1: α,α-dibromo-1-phenylethanone With dimethyl sulfoxide T=70 - 75°C; Inert atmosphere; 2: ethanol T=25 - 30°C; Inert atmosphere;
参考文献
Raghunadh, Akula; Meruva, Suresh Babu; Kumar, Nuka Anil; Kumar, Gudla Santosh; Rao, L. Vaikunta; Syamkumar
Synthesis, 2012 , vol. 2012, # 2 p. 283 - 289
反应条件
1: α,α-dibromo-1-phenylethanone With dimethylsulfoxide-d6 T=70 - 75°C; Inert atmosphere; 2: methanol-d4 T=25 - 30°C; Inert atmosphere;
参考文献
Raghunadh, Akula; Meruva, Suresh Babu; Kumar, Nuka Anil; Kumar, Gudla Santosh; Rao, L. Vaikunta; Syamkumar
Synthesis, 2012 , vol. 2012, # 2 p. 283 - 289
反应条件
Oxonereg;; potassium bromide in water; acetonitrile
T=20°C; 0.25 h; Reagent/catalyst;
参考文献
Madabhushi, Sridhar; Jillella, Raveendra; Mallu, Kishore Kumar Reddy; Godala, Kondal Reddy; Vangipuram, Venkata Sairam
Tetrahedron Letters, 2013 , vol. 54, # 30 p. 3993 - 3996
反应条件
carbon tetrabromide; hydrogen bromide; oxygen in water; ethyl acetate
T=40°C; Irradiation;
参考文献
Tada, Norihiro; Ban, Kazunori; Ishigami, Takafumi; Nobuta, Tomoya; Miura, Tsuyoshi; Itoh, Akichika
Tetrahedron Letters, 2011 , vol. 52, # 29 p. 3821 - 3824
反应条件
Galden HT135; bromine; potassium carbonate in chloroform
T=20°C; 46 h;
参考文献
Kawakami, Kazumitsu; Tsuda, Akihiko
Chemistry - An Asian Journal, 2012 , vol. 7, # 10 p. 2240 - 2252
反应条件
hydrogen bromide; bromine; oxygen in water; ethyl acetate
10 h; Irradiation;
参考文献
Tada, Norihiro; Ban, Kazunori; Ishigami, Takafumi; Nobuta, Tomoya; Miura, Tsuyoshi; Itoh, Akichika
Tetrahedron Letters, 2011 , vol. 52, # 29 p. 3821 - 3824
反应条件
hydrogen bromide; dihydrogen peroxide in water; acetic acid
T=15 - 106°C; 0.333333 h;
参考文献
Terentev, Alexander O.; Krylov, Igor B.; Vil, Vera A.; Pastukhova, Zhanna Yu.; Fastov, Sergey A.; Nikishin, Gennady I.
Central European Journal of Chemistry, 2012 , vol. 10, # 2 p. 360 - 367
反应条件
N-bromosuccinmide in methanol
T=60 - 65°C; 0.3 h; SolventTemperatureTime;
参考文献
Mohan, Reddy Bodireddy; Reddy, N. C. Gangi
Synthetic Communications, 2013 , vol. 43, # 19 p. 2603 - 2614
