1-(4-溴苯肼)-2-苯乙炔合成路线 （共 49 条）
反应条件
sodium hydroxide; palladium diacetate in water; acetone
T=60°C; Sonogashira reaction; 1 h;
参考文献
Shi, Shengyin; Zhang, Yuhong
Synlett, 2007 , # 12 p. 1843 - 1850
反应条件
2,6-dimethylpyridine; oxygen; copper(I) bromide in methanol
T=45°C; Sonogashira coupling; P=760.051 Torr; 16 h;
参考文献
Yasukawa, Tomohiro; Miyamura, Hiroyuki; Kobayashi, Sh
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 18 p. 6208 - 6210
反应条件
copper(l) iodide; [Pt(PPh3)4] in N,N-dimethyl-formamide
T=120°C; 15 h;
参考文献
Oh, Chang Ho; Reddy, V. Raghava
Synlett, 2004 , # 12 p. 2091 - 2094
反应条件
triethylamine; AgCl; palladium dichloride in acetonitrile
T=20°C; Sonogashira coupling; 0.583333 h;
参考文献
Zhu, Min; Zhou, Zhongshi; Chen, Rui
Synthesis, 2008 , # 17 art. no. P04108SS, p. 2680 - 2682
反应条件
KOC(O)Ph; triphenylphosphine; copper(l) chloride in 1,3-dimethyl-imidazolidin-2-one
T=120°C; Sila-Sonogashira-Hagihara cross-coupling reaction; 12 h; Inert atmosphere;
参考文献
Ihara, Hideki; Ueda, Akinori; Suginome, Michinori
Chemistry Letters, 2011 , vol. 40, # 9 p. 972 - 974
反应条件
copper(l) iodide; 8-hydroxy-quinoline; potassium carbonate in N,N-dimethyl-formamide
T=110°C; 24 h; Inert atmosphere;
参考文献
Yan, Hong; Lu, Linhua; Sun, Peng; Zhu, Yan; Yang, Hailong; Liu, Defu; Rong, Guangwei; Mao, Jincheng
RSC Advances, 2013 , vol. 3, # 2 p. 377 - 381
反应条件
copper; zinc; bis(cyclopentadienyl)titanium dichloride; bis-triphenylphosphine-palladium(II) chloride in ethylene glycol dimethyl ether
T=65°C; 5 h;
参考文献
Tamaru, Yoshinao; Ochiai, Hirofumi; Yoshida, Zen-ichi
Tetrahedron Letters, 1984 , vol. 25, # 35 p. 3861 - 3864
反应条件
carbon monoxide; copper; zinc; bis(cyclopentadienyl)titanium dichloride; bis-triphenylphosphine-palladium(II) chloride in ethylene glycol dimethyl ether
T=65°C; 5 h;
参考文献
Tamaru, Yoshinao; Ochiai, Hirofumi; Yoshida, Zen-ichi
Tetrahedron Letters, 1984 , vol. 25, # 35 p. 3861 - 3864
反应条件
potassium hydroxide in ethanol
T=110°C; 24 h;
参考文献
Hellwinkel, Dieter; Fritsch, Helmut
Chemische Berichte, 1989 , vol. 122, p. 2351 - 2360
反应条件
copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride in toluene
T=80°C; Sonogashira coupling; 24 h;
参考文献
Chow; Wan; Low; Yeung
Journal of Organic Chemistry, 2001 , vol. 66, # 5 p. 1910 - 1913
