1,4-双(2-噻吩基)-1,4-丁二酮合成路线 （共 28 条）
反应条件
ethylaluminum dichloride in dichloromethane T=0°C; 2 h; Inert atmosphere;
参考文献
Uenver, Halil; Biyikoglu, Mutluhan; Bulut, Adnan
Asian Journal of Chemistry, 2013 , vol. 25, # 15 p. 8772 - 8774
反应条件
sodium naphthalenide in tetrahydrofuran T=0 - 5°C; 2 h;
参考文献
Banerji, Avijit; Bandyopadhyay, Debasish; Basak, Bidyut; Sur, Kumar R.; Paul, Jyoti N.; Banerji, Julie; Chatterjee, Asima
Tetrahedron Letters, 2005 , vol. 46, # 41 p. 7033 - 7035
反应条件
sodium acetate; 3,4-dimethyl-5-(2-hydroxyethyl)-thiazolium iodide in ethanol 1) 3 h, 80 deg C, 2) 12 h, reflux;
参考文献
Kaiser; Behl; Schroeter; Kratz; Lendlein
Reactive and Functional Polymers, 2012 , vol. 72, # 8 p. 533 - 541
反应条件
oxalic acid in tetrahydrofuran 1.5 h; Heating;
参考文献
Takahashi, Kazumasa; Matsuzaki, Masahiro; Ogura, Katsuyuki; Iida, Hirotada
Journal of Organic Chemistry, 1983 , vol. 48, # 11 p. 1909 - 1912
反应条件
[Ru(tris(2,2'-bipyridyl))3]Cl2·6H2O; potassium carbonate; triethylamine in acetonitrile T=20°C; 14 h; Schlenk techniqueIrradiation;
参考文献
Xuan, Jun; Feng, Zhu-Jia; Chen, Jia-Rong; Lu, Liang-Qiu; Xiao, Wen-Jing
Chemistry - A European Journal, 2014 , vol. 20, # 11 p. 3045 - 3049
反应条件
lead(IV) acetate in tetrahydrofuran; dichloromethane T=-78 - -25°C; 2.5 h; 1) -78 degC, 1.5h 2) R.T., 1h;
参考文献
Moriarty, Robert M.; Penmasta, Raju; Prakash, Indra
Tetrahedron Letters, 1987 , vol. 28, # 8 p. 873 - 876
反应条件
sodium cyanide in N,N-dimethyl-formamide
参考文献
Wynberg, Hans; Metselaar, Jan
Synthetic Communications, 1984 , vol. 14, # 1 p. 1 - 10
反应条件
iodosylbenzene; boron trifluoride diethyl etherate in dichloromethane 1.) -40 deg C, 1 h; 2.) room temp., 1 h;
参考文献
Moriarty, Robert; Prakash, Om; Duncan, Michael P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 559 - 562
反应条件
aluminium trichloride in 1,2-dichloro-ethane T=16 - 20°C; 4.5 h; Yields of byproduct given;
参考文献
Merz; Ellinger
Synthesis, 1991 , # 6 p. 462 - 464
反应条件
copper dichloride; lithium diisopropyl amide 1.) hexane, THF, -78 deg C, 30 min, 2.) DMF, hexane, THF, -40 deg C, 40 min; Yield given. Multistep reaction;
参考文献
Heterocycles, , vol. 20, # 10 p. 1941 - 1943
