1,4-双(2-噻吩基)-1,4-丁二酮合成路线 (共 28 条)
反应条件
triethylamine in tetrahydrofuran 8 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 8 p. 905 - 912
反应条件
2: 93 percent / 30percent aq. oxalic acid / tetrahydrofuran / 1.5 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 48, # 11 p. 1909 - 1912
反应条件
AlCl3, aluminium chloride in dichloromethane T=40°C; 12 h;
参考文献
Smirnov; Afanas'Ev; Belen'kii
Chemistry of Heterocyclic Compounds, 2011 , vol. 46, # 10 p. 1199 - 1207
反应条件
AlCl3, aluminium chloride in dichloromethane T=20°C; 3 h;
参考文献
Chemistry of Heterocyclic Compounds, , vol. 46, # 10 p. 1199 - 1207
反应条件
iodosylbenzene; boron trifluoride diethyl etherate in water 0-5 deg C, 2 h then r.t., 2 days;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1781 - 1784
反应条件
tributylphosphine in tetrahydrofuran 10 h; Ambient temperature;
参考文献
Ohta, Akira; Kobayashi, Tomoshige; Kato, Hiroshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 8 p. 905 - 912
反应条件
AlCl3, aluminium chloride in dichloromethane T=20°C; 3 h;
参考文献
Chemistry of Heterocyclic Compounds, , vol. 46, # 10 p. 1199 - 1207
反应条件
1: ammonium hydroxide / ethanol 2: sodium cyanide View Scheme
参考文献
Russian Journal of Applied Chemistry, , vol. 83, # 8 p. 1440 - 1443
反应条件
in diethyl ether 24 h; Ambient temperature;
参考文献
Leung, Wai-Yee; LeGoff, Eugene
Synthetic Communications, 1989 , vol. 19, # 5and6 p. 787 - 792
反应条件
titanium(IV) isopropylate; 1,4-dioxane dibromide 1) ether, 2) CCl4, 20 deg C, 7 d; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Russian Journal of Organic Chemistry, , vol. 31, # 8 p. 1060 - 1062
Zhurnal Organicheskoi Khimii, , vol. 31, # 8 p. 1166 - 1168