1: With methanesulfonic acid T=55°C; 24 h; 2: With sodium hydrogencarbonate in water T=10°C; pH=4.5; 3: With sodium hydrogencarbonate more than 3 stages;
(R)-N-dicyclohexylphosphino-N-methyl-[(S)-2-(diphenylphosphino)ferrocenyl]ethylamine; hydrogen; bis(cycloocta-1,5-diene)rhodium(I) trifluoromethanesulfonate in tetrahydrofuran T=25°C; P=15514.4 Torr; 6 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 70, # 5 p. 1872 - 1880