1H-吡啶并[2,3-b][1,4]噁嗪-2(3h)-酮合成路线 (共 4 条)
反应条件
potassium carbonate in acetonitrile T=20°C; Heating;
参考文献
Ahn, Sung Oh; Park, Chan Hee; Im, Jun Hwan; Lee, Soon Ok; Lee, Kyoung June; Cho, Seong Wook; Ko, Kwang Seok; Han, Sun Young; Lee, Won Il
Patent: US2011/28467 A1, 2011 ;
Location in patent: Page/Page column 14 ;
US 20110028467 A1
反应条件
acetic acid T=60°C; 0.166667 h;
参考文献
WO2010/116270 A1, ;
Page/Page column 85-86 ;
WO 2010/116270 A1
反应条件
caesium carbonate T=130°C; 0.333333 h; Microwave irradiation;
参考文献
Lim, Jae-Min; Gam, Gyunghee; Kim, Shin-Hyuong; Shin, Dong-Soo; Jang, Kiwan
Journal of the Korean Chemical Society, 2012 , vol. 56, # 4 p. 468 - 472,5
Title/Abstract Full Text Show Details
Lim, Jae-Min; Gam, Gyunghee; Kim, Shin-Hyuong; Jang, Kiwan; Shin, Dong-Soo
Journal of the Korean Chemical Society, 2012 , vol. 56, # 4 p. 468 - 472
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran T=0 - 20°C; 2: With sodium hydroxide in tetrahydrofuran; water
参考文献
Ahn, Sung Oh; Park, Chan Hee; Im, Jun Hwan; Lee, Soon Ok; Lee, Kyoung June; Cho, Seong Wook; Ko, Kwang Seok; Han, Sun Young; Lee, Won Il
Patent: US2011/28467 A1, 2011 ;
Location in patent: Page/Page column 14 ;
US 20110028467 A1