反应条件
1.1: 85 percent / sodium iodide / acetone / Heating 2.1: zinc; 1,2-dibromoethane; chlorotrimethylsilane / tetrahydrofuran / 30 - 68 °C 2.2: CuCN; LiCl / tetrahydrofuran / -14 °C 2.3: tetrahydrofuran; diethyl ether / 37 h / -78 - 20 °C 3.1: 2.9 g / aq. HCl / ethanol / 0.25 h / 20 °C 4.1: 87 percent / aq. KOH / ethanol / 3 h View Scheme
参考文献
Toshima, Hiroaki; Nara, Shinji; Aramaki, Hisateru; Ichihara, Akitami; Koda, Yasunori; Kikuta, Yoshio
Bioscience, Biotechnology and Biochemistry, 1997 , vol. 61, # 10 p. 1724 - 1728
