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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3-苯基呋喃
合成路线
（共 31 条）
55552-70-0
3-呋喃硼酸
+
16156-59-5
甲磺酸苯酯
→
反应条件
13679-41-9
3-苯基呋喃
反应条件
potassium phosphate; 1-methyl-2-(2-(dicyclohexylphosphino)phenyl)-1H-benzoimidazole; palladium diacetate in tert-butyl alcohol T=20 - 120°C; Suzuki-Miyaura coupling; 24 h;
参考文献
Chung, Kin Ho; So, Chau Ming; Wong, Shun Man; Luk, Chi Him; Zhou, Zhongyuan; Lau, Chak Po; Kwong, Fuk Yee
Chemical Communications, 2012 , vol. 48, # 14 p. 1967 - 1969
84735-60-4
→
反应条件
13679-41-9
3-苯基呋喃
反应条件
nickel in ethanol; acetone 0.5 h; Ambient temperature;
参考文献
Okazaki, Renji; Negishi, Yoshio; Inamoto, Naoki
Journal of the Chemical Society, Chemical Communications, 1982 , # 18 p. 1055 - 1056
22037-28-1
3-溴呋喃
+
166328-07-0
(1-萘)三氟硼酸钾
→
反应条件
13679-41-9
3-苯基呋喃
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; triethylamine in ethanol Suzuki-Miyaura cross-coupling; 9 h; Heating;
参考文献
Molander, Gary A.; Biolatto, Betina
Journal of Organic Chemistry, 2003 , vol. 68, # 11 p. 4302 - 4314
591-50-4
碘苯
→
反应条件
13679-41-9
3-苯基呋喃
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran 10 h; Ambient temperature;
参考文献
Negishi, Ei-ichi; Luo, Fen-Tair; Frisbee, Roger; Matsushita, Hajime
Heterocycles, 1982 , vol. 18, p. 117 - 122
201230-82-2
+
1504-58-1
3-苯基-2-丙炔-1-醇
→
反应条件
13679-41-9
3-苯基呋喃
反应条件
hydrogen; triphenylphosphine; dirhodium tetraacetate in dichloromethane T=65°C; P=36200.4 Torr; 24 h; Product distribution; Further Variations:ReagentsSolventsTemperaturescatalyst/ligand ratio;
参考文献
Nanayakkara, Peru; Alper, Howard
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 4-5 p. 545 - 550
6006-81-1
beta-亚甲基苯乙醇
→
反应条件
13679-41-9
3-苯基呋喃
反应条件
1.1: 75 percent / dppp; Et3N / Pd(OAc)2 / acetonitrile / Heating 2.1: Pcy3Cl2Ru=CHPh(diMesIm) / CH2Cl2 / Heating 2.2: 70 percent / TFA / CH2Cl2 / 20 °C View Scheme
参考文献
Donohoe, Timothy J.; Orr, Allan J.; Gosby, Katherine; Bingham, Matilda
European Journal of Organic Chemistry, 2005 , # 10 p. 1969 - 1971
13636-88-9
3,3-双甲基磺酰基-1-苯丙酮
→
反应条件
13679-41-9
3-苯基呋喃
反应条件
1: 92 percent / tetrahydrofuran / 1 h, -70 deg C, than 1 h, r.t. 2: 91 percent / HCl / methanol; H2O / 1 h / Ambient temperature 3: 42 percent / Raney Ni / ethanol / 0.5 h / Ambient temperature View Scheme
参考文献
Okazaki, Renji; Negishi, Yoshio; Inamoto, Naoki
Journal of the Chemical Society, Chemical Communications, 1982 , # 18 p. 1055 - 1056
84735-55-7
→
反应条件
13679-41-9
3-苯基呋喃
反应条件
1: 91 percent / HCl / methanol; H2O / 1 h / Ambient temperature 2: 42 percent / Raney Ni / ethanol / 0.5 h / Ambient temperature View Scheme
参考文献
Okazaki, Renji; Negishi, Yoshio; Inamoto, Naoki
Journal of the Chemical Society, Chemical Communications, 1982 , # 18 p. 1055 - 1056
6956-56-5
→
反应条件
13679-41-9
3-苯基呋喃
反应条件
1: 75 percent / t-BuOK / tetrahydrofuran / -40 °C 2: HCl / Ambient temperature View Scheme
参考文献
Buxton, Sheila R.; Holm, Kjetil H.; Skattebol, Lars
Tetrahedron Letters, 1987 , vol. 28, # 19 p. 2167 - 2168
591-50-4
碘苯
→
反应条件
13679-41-9
3-苯基呋喃
反应条件
1: diisopropylethylamine; benzyltriethylammonium chloride; palladium(II) acetate / dimethylformamide / 6 h / 80 °C 2: 35 percent hydroperchloric acid / tetrahydrofuran / 48 h / Heating 3: 89 percent / diisobutylaluminum hydride / toluene; CH2Cl2 / -78 °C View Scheme
参考文献
Taniguchi, Takahiko; Nagata, Hiroshi; Kanada, Regina Mikie; Kadota, Kohei; Takeuchi, Miwako; Ogasawara, Kunio
Heterocycles, 2000 , vol. 52, # 1 p. 67 - 71
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