4-(5-甲基-2-呋喃)丁烷-2-酮合成路线 （共 20 条）
反应条件
magnesium in tetrahydrofuran; methanol
参考文献
Waidmann, Christopher R.; Pierpont, Aaron W.; Batista, Enrique R.; Gordon, John C.; Martin, Richard L.; Pete Silks; West, Ryan M.; Wu, Ruilian
Catalysis Science and Technology, 2013 , vol. 3, # 1 p. 106 - 115
反应条件
acetic acid; hydroquinone in water T=130°C; 0.666667 h;
参考文献
Kouridaki, Antonia; Montagnon, Tamsyn; Tofi, Maria; Vassilikogiannakis, Georgios
Organic Letters, 2012 , vol. 14, # 9 p. 2374 - 2377
反应条件
oxygen; palladium diacetate in acetic acid T=50°C; Heck Reaction; P=760.051 Torr; Schlenk technique;
参考文献
Huang, Liangbin; Qi, Ji; Wu, Xia; Wu, Wanqing; Jiang, Huanfeng
Chemistry - A European Journal, 2013 , vol. 19, # 46 p. 15462 - 15466
反应条件
methanol; magnesium in tetrahydrofuran
参考文献
Dominguez, Carmen; Csaky, Aurelio G.; Plumet, Joaquin
Tetrahedron Letters, 1991 , vol. 32, # 33 p. 4183 - 4184
反应条件
boron trifluoride diethyl etherate in diethyl ether; nitromethane T=-20°C; 1 h;
参考文献
Poirier, Jean-Marie; Dujardin, Gilles
Heterocycles, 1987 , vol. 25, p. 399 - 407
反应条件
in various solvent(s) T=30°C; Diels-Alder reaction; P=2250180 Torr; 16 h;
参考文献
Jenner, Gerard; Gacem, Badra
Journal of Physical Organic Chemistry, 2003 , vol. 16, # 5 p. 265 - 270
反应条件
1: aq. NaOH solution 2: palladium; methanol / Hydrogenation View Scheme
参考文献
Sutton, Andrew D.; Waldie, Fraser D.; Wu, Ruilian; Schlaf, Marcel; 'Pete'Silks, Louis A.; Gordon, John C.
Nature Chemistry, 2013 , vol. 5, # 5 p. 428 - 432
反应条件
magnesium silicate T=25°C; 70 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Veselovskii, V. V.; Gybin, A. S.; Lozanova, A. V.; Moiseenkov, A. M.; Smit, V. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 1.1 p. 94 - 100
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 1 p. 107 - 113
反应条件
1: piperidine 2: magnesium / tetrahydrofuran; methanol 3: hydrogenchloride / methanol; water / 24 h / 80 °C 4: magnesium / tetrahydrofuran; methanol View Scheme
参考文献
Waidmann, Christopher R.; Pierpont, Aaron W.; Batista, Enrique R.; Gordon, John C.; Martin, Richard L.; Pete Silks; West, Ryan M.; Wu, Ruilian
Catalysis Science and Technology, 2013 , vol. 3, # 1 p. 106 - 115
反应条件
1: hydrogenchloride / methanol; water / 24 h / 80 °C 2: magnesium / tetrahydrofuran; methanol View Scheme
参考文献
Waidmann, Christopher R.; Pierpont, Aaron W.; Batista, Enrique R.; Gordon, John C.; Martin, Richard L.; Pete Silks; West, Ryan M.; Wu, Ruilian
Catalysis Science and Technology, 2013 , vol. 3, # 1 p. 106 - 115
