氯二[4-(三氟甲基)苯基]膦合成路线 （共 8 条）
反应条件
hydrogenchloride in tetrahydrofuran; cyclohexane
参考文献
Journal of the American Chemical Society, , vol. 116, # 22 p. 9869 - 9882
参考文献
Organic Letters, , vol. 6, # 25 p. 4675 - 4678
反应条件
phosphorus trichoride in dichloromethane 1.5 h;
参考文献
Journal of the American Chemical Society, , vol. 116, # 22 p. 9869 - 9882
反应条件
1: With magnesium in tetrahydrofuran T=20°C; Grignard reaction; 2 h; 2: With N,N-diethylphosphoramidous dichloride in tetrahydrofuran T=0 - 50°C; phosphorylation; 3 h; 3: With hydrogenchloride in pentane T=0°C; Hydrolysis; 1 h;
参考文献
Tetrahedron Asymmetry, , vol. 10, # 17 p. 3341 - 3352
反应条件
pyridine; magnesium 1.) ether, reflux, 2 h, 2.) r.t., overnight; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 60, # 11 p. 3499 - 3508
参考文献
Pu, Xiaotao; Qi, Xiangbing; Ready, Joseph M.
Journal of the American Chemical Society, 2009 , vol. 131, # 30 p. 10364 - 10365
反应条件
in tetrahydrofuran; diethyl ether
T=-5 - 23°C;
参考文献
Gulyas, Henrik; Bacsik, Zoltan; Szoellosy, Aron; Bakos, Jozsef
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 10-11 p. 1306 - 1310
反应条件
in toluene
3 h; Reflux;
参考文献
Teng, Ming-Yu; Zhang, Song; Jin, Yi-Ming; Li, Tian-Yi; Liu, Xuan; Xu, Qiu-Lei; Lin, Chen; Zheng, You-Xuan; Wang, Leyong; Zuo, Jing-Lin
Dyes and Pigments, 2014 , vol. 105, p. 105 - 113
