9,9-二甲基-9H-9-硅芴合成路线 （共 43 条）
反应条件
aluminium trichloride; dimethyl-dichlorosilane 4 h; Heating;
参考文献
Chernyshev, E. A.; Komalankova, N. G.; Shashkov, I. A.; Nosova, V. M.; Silkina, N. N.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 7 p. 1607 - 1613,1432 - 1437
反应条件
1,4-diaza-bicyclo[2.2.2]octane; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in 1,4-dioxane; water
T=100°C; 15 h; oilbathInert atmosphere;
参考文献
Tobisu, Mamoru; Onoe, Masahiro; Kita, Yusuke; Chatani, Naoto
Journal of the American Chemical Society, 2009 , vol. 131, p. 7506 - 7507
反应条件
1: 2,2'-dibromobiphenyl With n-butyllithium in diethyl ether; hexane
T=-78 - 20°C;
2: dimethyl-dichlorosilane in diethyl ether; hexane
T=-78 - 20°C; Further stages.;
参考文献
Liu; Stringfellow; Ballweg; Guzei; West
Journal of the American Chemical Society, 2002 , vol. 124, # 1 p. 49 - 57
反应条件
bis(η3-allyl-μ-chloropalladium(II)); tri-tert-butyl phosphine; 4-nitrobenzaldehdye; lithium tert-butylate in toluene
T=120°C; 10 h; Inert atmosphere;
参考文献
Ouyang, Kunbing; Liang, Yun; Xi, Zhenfeng
Organic Letters, 2012 , vol. 14, # 17 p. 4572 - 4575
反应条件
di-tert-butyl peroxide
T=130°C; 2 h;
参考文献
Kira,M.; Sakamoto,K.; Sakurai,H.
Journal of the American Chemical Society, 1983 , vol. 105, p. 7469
反应条件
in benzene
5 h; Irradiation;
参考文献
Kira,M.; Sakamoto,K.; Sakurai,H.
Journal of the American Chemical Society, 1983 , vol. 105, p. 7469
反应条件
Wilkinson's catalyst in 1,4-dioxane
T=135°C; 0.25 h; Inert atmosphere;
参考文献
Ureshino, Tomonari; Yoshida, Takuya; Kuninobu, Yoichiro; Takai, Kazuhiko
Journal of the American Chemical Society, 2010 , vol. 132, # 41 p. 14324 - 14326
反应条件
in benzene
5 h; Irradiation;
参考文献
Kira,M.; Sakamoto,K.; Sakurai,H.
Journal of the American Chemical Society, 1983 , vol. 105, p. 7469
反应条件
1: 2,2'-dibromobiphenyl With tert.-butyl lithium in tetrahydrofuran; pentane
T=-75 - -60°C; 1 h;
2: benzylchlorodimethylsilane With triethylamine in tetrahydrofuran; pentane
T=20°C; 1.5 h;
参考文献
Hudrlik, Paul F.; Dai, Donghua; Hudrlik, Anne M.
Journal of Organometallic Chemistry, 2006 , vol. 691, # 6 p. 1257 - 1264
反应条件
in tetrahydrofuran
T=20°C;
参考文献
Liu; Stringfellow; Ballweg; Guzei; West
Journal of the American Chemical Society, 2002 , vol. 124, # 1 p. 49 - 57
