9,9-二甲基-9H-9-硅芴合成路线 （共 43 条）
反应条件
in tetrahydrofuran
72 h; Ambient temperature;
参考文献
Neugebauer, Wolfgang; Kos, Alexander J.; Schleyer, Rague
Journal of Organometallic Chemistry, 1982 , vol. 228, # 2 p. 107 - 118
反应条件
magnesium in tetrahydrofuran
168 h; Heating; Yield given. Title compound not separated from byproducts;
参考文献
Corey, J. Y.; McCarthy, W. Z.
Journal of Organometallic Chemistry, 1984 , vol. 271, # 1-3 p. 319 - 326
反应条件
magnesium; iodine
1.) THF, 6 h, 2.) THF, r.t.; Yield given. Multistep reaction;
参考文献
Corey, Joyce Y.; Chang, Lihsueh S.
Journal of Organometallic Chemistry, 1986 , vol. 307, p. 7 - 14
反应条件
lithium in tetrahydrofuran
Substitution; dimerization;
参考文献
Choi; Boudjouk
Tetrahedron Letters, 2000 , vol. 41, # 35 p. 6685 - 6688
参考文献
Gilman; Gorsich
Journal of the American Chemical Society, 1958 , vol. 80, p. 1883,1884
参考文献
Gilman; Gorsich
Journal of the American Chemical Society, 1958 , vol. 80, p. 3243,3244
反应条件
in benzene
Ambient temperatureIrradiationvar. solv.: hexane; add of 2,3-dimethylbutadiene; Yield given;
参考文献
Sakurai, Hideki; Sakamoto, Kenkichi; Kira, Mitsuo
Chemistry Letters, 1984 , p. 1379 - 1382
参考文献
Corey, Joyce Y.; Jonh, Christy S.; Ohmsted, Martha C.; Chang, Lihsueh S.
Journal of Organometallic Chemistry, 1986 , vol. 304, p. 93 - 106
反应条件
in tetrahydrofuran; diethyl ether
1 h; Ambient temperature;
参考文献
Ishikawa, Mitsuo; Tabohashi, Tatsuru; Sugisawa, Hiroshi; Nishimura, Kunio; Kumada, Makoto
Journal of Organometallic Chemistry, 1983 , vol. 250, # 1 p. 109 - 120
反应条件
in tetrahydrofuran; diethyl ether
1 h; Ambient temperature;
参考文献
Ishikawa, Mitsuo; Tabohashi, Tatsuru; Sugisawa, Hiroshi; Nishimura, Kunio; Kumada, Makoto
Journal of Organometallic Chemistry, 1983 , vol. 250, # 1 p. 109 - 120
