您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
13688-78-3
合成路线
（共 10 条）
13688-78-3
→
反应条件
49742-56-5
4’-甲基[1,1’-联苯]-4-甲酸甲酯
反应条件
tri-tert-butyl phosphine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in ethylene glycol dimethyl ether; hexane T=20°C;
参考文献
Saeki, Tomoyuki; Matsunaga, Tadafumi; Son, Eun-Cheol; Tamao, Kohei
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1689 - 1692
13688-78-3
→
反应条件
5748-38-9
4-乙酰基-4'-甲基联苯
反应条件
tri-tert-butyl phosphine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in ethylene glycol dimethyl ether; hexane T=20°C;
参考文献
Saeki, Tomoyuki; Matsunaga, Tadafumi; Son, Eun-Cheol; Tamao, Kohei
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1689 - 1692
13688-78-3
+
99-91-2
对氯苯乙酮
→
反应条件
5748-38-9
4-乙酰基-4'-甲基联苯
反应条件
1: trifluoro(p-tolyl)silane With tetrabutyl ammonium fluoride; palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tert-butyl alcohol T=20°C; Hiyama cross-coupling reaction; 0.0833333 h; Inert atmosphereSealed vial; 2: para-chloroacetophenone in tert-butyl alcohol T=60°C; Hiyama cross-coupling reaction; Inert atmosphereSealed vial;
参考文献
Molander, Gary A.; Iannazzo, Laura
Journal of Organic Chemistry, 2011 , vol. 76, # 21 p. 9182 - 9187
13688-78-3
+
1104800-72-7
→
反应条件
53040-92-9
4-甲氧基-4-甲基-联苯
反应条件
tri-tert-butyl phosphine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in ethylene glycol dimethyl ether; hexane T=20°C; 18 h; Product distribution; Further Variations:CatalystsReagents;
参考文献
Advanced Synthesis and Catalysis, , vol. 346, # 13-15 p. 1689 - 1692
13329-40-3
4-碘代苯乙酮
+
201230-82-2
+
13688-78-3
→
反应条件
586-89-0
4-乙酰基苯甲酸
+
127118-95-0
反应条件
potassium fluoride; bis(η3-allyl-μ-chloropalladium(II)) T=100°C; P=760 Torr;
参考文献
Chemistry Letters, , p. 2049 - 2052
62499-16-5
+
13688-78-3
→
反应条件
19482-11-2
反应条件
tri-tert-butyl phosphine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in ethylene glycol dimethyl ether; hexane T=20°C;
参考文献
Saeki, Tomoyuki; Matsunaga, Tadafumi; Son, Eun-Cheol; Tamao, Kohei
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1689 - 1692
13688-78-3
→
反应条件
72093-43-7
4-氟-4-甲基-1,1-联苯
反应条件
tri-tert-butyl phosphine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in ethylene glycol dimethyl ether; hexane T=20°C;
参考文献
Saeki, Tomoyuki; Matsunaga, Tadafumi; Son, Eun-Cheol; Tamao, Kohei
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1689 - 1692
13688-78-3
→
反应条件
7383-90-6
3,4'-二甲基-1,1'-联苯
反应条件
tri-tert-butyl phosphine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in ethylene glycol dimethyl ether; hexane T=20°C;
参考文献
Saeki, Tomoyuki; Matsunaga, Tadafumi; Son, Eun-Cheol; Tamao, Kohei
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1689 - 1692
21120-91-2
1-溴苯并环丁烯
+
13688-78-3
→
反应条件
661476-70-6
反应条件
[NiCl2(1,2-dimethoxyethane)]; (+)-Norephedrine; lithium hexamethyldisilazane; water; cesium fluoride in N,N-dimethyl acetamide T=60°C; Hiyama cross-coupling; 16 h;
参考文献
Strotman, Neil A.; Sommer, Stefan; Fu, Gregory C.
Angewandte Chemie - International Edition, 2007 , vol. 46, # 19 p. 3556 - 3558
13688-78-3
→
反应条件
611-61-0
2,4'-二甲基联苯
反应条件
tri-tert-butyl phosphine; tris(dibenzylideneacetone)dipalladium(0) chloroform complex in ethylene glycol dimethyl ether; hexane T=20°C;
参考文献
Saeki, Tomoyuki; Matsunaga, Tadafumi; Son, Eun-Cheol; Tamao, Kohei
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1689 - 1692
