1-(4-硝基苯基)-2-吡咯烷酮合成路线 (共 11 条)
反应条件
carbon tetrabromide; triphenylphosphine in acetonitrile T=60°C; 3 h;
参考文献
Yang, Yong-Hua; Shi, Min
Journal of Organic Chemistry, 2005 , vol. 70, # 21 p. 8645 - 8648
反应条件
1: CH2Cl2 / 78 h / 50 °C 2: Ph3P, Et3N / CH2Cl2 / 2 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 44, p. 3025
反应条件
sulfuric acid; nitric acid
参考文献
Justus Liebigs Annalen der Chemie, , vol. 596, p. 1,204
反应条件
1: 3 h / 200 - 210 °C 2: H2SO4 / 2 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 44, p. 3025
反应条件
sodium hydroxide in methanol; water T=25°C; KineticsEquilibrium constantActivation energy; Further Variations:Temperaturesreagent concentration;
参考文献
Journal of Physical Organic Chemistry, , vol. 15, # 3 p. 165 - 173
反应条件
hydrogenchloride; potassium chloride T=50°C; -ΔH0; -ΔS0; different temperatures and HCl concentrations; hydrogen isotope effect; KineticsEquilibrium constantThermodynamic data;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1243 - 1250
参考文献
WO2004/101557 A1, ;
Page/Page column 31 ;
反应条件
1: mixed acid 2: 2 M aq. NaOH / 0.5 h / Ambient temperature View Scheme
参考文献
Abdallah, Jassim M.; Moodie, Roy B.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 1243 - 1250
反应条件
water T=20°C; Inert atmosphere; chemoselective reaction;
参考文献
Dey, Raju; Mukherjee, Nirmalya; Ahammed, Sabir; Ranu, Brindaban C.
Chemical Communications, 2012 , vol. 48, # 64 p. 7982 - 7984
参考文献
Sedlak, Milos; Hejtmankova, Ludmila; Kasparova, Pavla; Kavalek, Jaromir
Journal of Physical Organic Chemistry, 2002 , vol. 15, # 3 p. 165 - 173