136918-14-4合成路线 （共 708 条）
反应条件
1: 20 °C / 600.05 Torr 2: 18 h / 20 °C / 0.8 Torr View Scheme
参考文献
Kaupp, Gerd; Schmeyers, Jens; Boy, Juergen
Tetrahedron, 2000 , vol. 56, # 36 p. 6899 - 6911
反应条件
pyridine; ethanol; trimethylphenylammonium hydroxide und Erwaermen des Reaktionsprodukts mit wss.HCl;
参考文献
Chimija chim.Technol.(NDVS)Chem.Abstr., , p. 545
Chimija chim.Technol.(NDVS)Chem.Abstr., , p. 2149
反应条件
hydrazine in ethanol T=5°C; 2 h;
参考文献
Dey, Sanjeev K.; Lightner, David A.
Journal of Organic Chemistry, 2007 , vol. 72, # 24 p. 9395 - 9397
反应条件
1: [bis(acetoxy)iodo]benzene / 2 h / 145 °C / Microwave irradiation 2: hydrazine hydrate / water; acetonitrile / 0.75 h / 20 °C View Scheme
参考文献
Kantak, Abhishek A.; Potavathri, Shathaverdhan; Barham, Rose A.; Romano, Kaitlyn M.; Deboef, Brenton
Journal of the American Chemical Society, 2011 , vol. 133, # 49 p. 19960 - 19965
反应条件
1: [bis(acetoxy)iodo]benzene / 3 h / 145 °C / Microwave irradiation 2: hydrazine hydrate / water; acetonitrile / 0.75 h / 20 °C View Scheme
参考文献
Kantak, Abhishek A.; Potavathri, Shathaverdhan; Barham, Rose A.; Romano, Kaitlyn M.; Deboef, Brenton
Journal of the American Chemical Society, 2011 , vol. 133, # 49 p. 19960 - 19965
反应条件
1: [bis(acetoxy)iodo]benzene / 3 h / 145 °C / Microwave irradiation 2: hydrazine hydrate / water; acetonitrile / 0.75 h / 20 °C View Scheme
参考文献
Kantak, Abhishek A.; Potavathri, Shathaverdhan; Barham, Rose A.; Romano, Kaitlyn M.; Deboef, Brenton
Journal of the American Chemical Society, 2011 , vol. 133, # 49 p. 19960 - 19965
反应条件
tetrahydrofuran; triphenylphosphine; diethylazodicarboxylate in toluene T=20°C; Mitsunobu reaction; 3 h; Inert atmosphere;
参考文献
Thvedt, Thor Hkon Krane; Fuglseth, Erik; Sundby, Eirik; Hoff, Brd Helge
Tetrahedron, 2010 , vol. 66, # 34 p. 6733 - 6743
反应条件
urea; Copper(I)chloride
参考文献
Ihara Chemical Industry Co., Ltd.
Patent: US4140695 A1, 1979 ;
反应条件
urea; Copper(I)chloride
参考文献
Ihara Chemical Industry Co., Ltd.
Patent: US4140695 A1, 1979 ;
反应条件
toluene-4-sulfonic acid; 1,1,1,3,3,3-hexamethyl-disilazane in N,N-dimethyl-formamide T=150°C; 10 h;
参考文献
Uchida, Hitoshi; Yoshiyama, Hideyuki; Reddy, Paidi Yella; Nakamura, Shuichi; Toru, Takeshi
Synlett, 2003 , # 13 p. 2083 - 2085
