136918-14-4合成路线 (共 708 条)
反应条件
potassium tert-butylate in dimethyl sulfoxide 5 h; Irradiation; Product distribution; Further Variations:Reagents;
参考文献
Maquieira, Manuel Bajo; Penenory, Alicia B.; Rossi, Roberto A.
Journal of Organic Chemistry, 2002 , vol. 67, # 3 p. 1012 - 1015
反应条件
1: With [bis(acetoxy)iodo]benzene T=145°C; 3 h; Microwave irradiation; 2: With hydrazine hydrate in water; acetonitrile
参考文献
Kantak, Abhishek A.; Potavathri, Shathaverdhan; Barham, Rose A.; Romano, Kaitlyn M.; Deboef, Brenton
Journal of the American Chemical Society, 2011 , vol. 133, # 49 p. 19960 - 19965
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran; toluene
参考文献
TAKEDA PHARMACEUTICAL COMPANY LIMITED
Patent: US2011/118172 A1, 2011 ;
反应条件
titanium tetrachloride; zinc in tetrahydrofuran T=0°C; 12 h;
参考文献
Kise, Naoki; Kawano, Yusuke; Sakurai, Toshihiko
Journal of Organic Chemistry, 2013 , vol. 78, # 24 p. 12453 - 12459
反应条件
potassium carbonate in methanol T=40°C; 12 h; Inert atmosphere;
参考文献
Islam, Sk.Manirul; Mondal, Sanchita; Mondal, Paramita; Roy, Anupam Singha; Tuhina; Salam, Noor; Mobarak, Manir
Journal of Organometallic Chemistry, 2012 , vol. 696, # 26 p. 4264 - 4274
反应条件
copper diacetate; oxygen; triethylamine; 4 A molecular sieve in dichloromethane T=45°C; 20 h;
参考文献
Chernick, Erin T.; Ahrens, Michael J.; Scheidt, Karl A.; Wasielewski, Michael R.
Journal of Organic Chemistry, 2005 , vol. 70, # 4 p. 1486 - 1489
反应条件
copper(I) oxide in various solvent(s) T=172°C; 24 h;
参考文献
Sato, Masaru; Ebine, Seiji; Akabori, Sadatoshi
Synthesis, 1981 , # 6 p. 472 - 473
反应条件
[bis(acetoxy)iodo]benzene T=145°C; 3 h; Microwave irradiation;
参考文献
Kantak, Abhishek A.; Potavathri, Shathaverdhan; Barham, Rose A.; Romano, Kaitlyn M.; Deboef, Brenton
Journal of the American Chemical Society, 2011 , vol. 133, # 49 p. 19960 - 19965
反应条件
pyridine; copper diacetate in dichloromethane T=40°C; 48 h;
参考文献
Rasmussen, L. Kyhn; Begtrup, Mikael; Ruhland, Thomas
Journal of Organic Chemistry, 2004 , vol. 69, # 20 p. 6890 - 6893
反应条件
pyridine; copper diacetate in dichloromethane 48 h; Ambient temperature;
参考文献
Chan, Dominic M. T.
Tetrahedron Letters, 1996 , vol. 37, # 50 p. 9013 - 9016