136918-14-4合成路线 （共 708 条）
反应条件
hydrazine in ethanol; dichloromethane
反应条件
sodium hydroxide; zinc Behandeln des Reaktionsprodukts mit Wasser, dann mit verd. Salzsaeure;
参考文献
Gardner; Naylor
Organic Syntheses, 1936 , vol. 16, p. 71
Organic Syntheses, 1943 , vol. Coll. Vol. II, p. 526
反应条件
titanium tetrachloride; potassium carbonate; zinc 1.) xylene, 110 deg C, 20 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Li, Jing; Chen, Jian; Chen, Hai-Bo; Chen, Wei-Xing
Synthetic Communications, 1998 , vol. 28, # 7 p. 1281 - 1286
反应条件
Kochen der mit Salzsaeure angesaeuerten Loesung;
参考文献
Ruggli; Meyer,E.
Helvetica Chimica Acta, 1922 , vol. 5, p. 31
Full Text Show Details
Kalle and Co.
Patent: DE267596 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 11, p. 196
Full Text Show Details
Reissert
Chemische Berichte, 1913 , vol. 46, p. 1488
反应条件
potassium carbonate in acetonitrile 12 h; Reflux;
参考文献
Lipshutz, Bruce H.; Ghorai, Subir; Leong, Wendy Wen Yi
Journal of Organic Chemistry, 2009 , vol. 74, # 7 p. 2854 - 2857
反应条件
1: With triphenylphosphine in tetrahydrofuran 2: With di-isopropyl azodicarboxylate in tetrahydrofuran T=0 - 20°C;
参考文献
Malkov, Andrei V.; Derrien, Nolwenn; Barlog, Maciej; Kocovsky, Pavel
Chemistry - A European Journal, 2014 , vol. 20, # 16 p. 4542 - 4547
反应条件
1.1: water / 4 h / 100 °C 2.1: thionyl chloride / 4 h / 75 °C / Inert atmosphere 3.1: sodium iodide / acetone / 4 h / 20 °C / Darkness 4.1: copper(l) iodide; diethylzinc / hexane; dichloromethane / 2 h / 20 °C / Inert atmosphere 4.2: 4 h / 20 °C / Inert atmosphere View Scheme
参考文献
Maury, Julien; Mouysset, Dominique; Feray, Laurence; Marque, Sylvain R. A.; Siri, Didier; Bertrand, Michele P.
Chemistry - A European Journal, 2012 , vol. 18, # 11 p. 3241 - 3247
反应条件
bis-(2-(1-adamantyl)ethyl) azodicarboxylate; triphenylphosphine Mitsunobu reaction;
参考文献
Tetrahedron Letters, , vol. 45, # 35 p. 6653 - 6656
反应条件
potassium hydroxide; 1-n-butyl-3-methylimidazolium tetrafluoroborate T=40°C; 5 h;
参考文献
Synthesis, , # 2 p. 208 - 212
