136918-14-4合成路线 （共 708 条）
反应条件
1: potassium carbonate; dimethylformamide / Beim Erhitzen des Reaktionsgemisches mit Benzoesaeure-<4-chlor-butylester> und Kaliumbromid 2: water; ethanol; hydrochloric acid View Scheme
参考文献
Bergmann; Kaluszyner
Recueil des Travaux Chimiques des Pays-Bas, 1959 , vol. 78, p. 289,309
反应条件
2.2.4.4.6.6-hexamethyl-2.4.6-trisila-3.5-dioxaheptane; tetrabutylammomium bromide; potassium carbonate 2 h; RefluxGreen chemistry; Solvent;
参考文献
Ab Rani, Mohd Azri; Borduas, Nadine; Colquhoun, Victoria; Hanley, Robert; Johnson, Henry; Larger, Solene; Lickiss, Paul D.; Llopis-Mestre, Veronica; Luu, Selina; Mogstad, Martin; Oczipka, Philipp; Sherwood, James R.; Welton, Tom; Xing, Jun-Yi
Green Chemistry, 2014 , vol. 16, # 3 p. 1282 - 1296
反应条件
2: concentrated sulfuric acid; hydrobromic acid / 50 - 60 °C View Scheme
参考文献
Pucher; Johnson
Journal of the American Chemical Society, 1922 , vol. 44, p. 823
反应条件
tin(IV) chloride 5 h; Heating;
参考文献
Szmigielski, Rafal; Danikiewicz, Witold
Synlett, 2003 , # 3 p. 372 - 376
反应条件
potassium carbonate; Methyl methyltrioctylammonium sulfate in toluene T=100°C; 4.5 h;
参考文献
Vasilevskaya; Grineva; Chernousova; Grankina; Andrievskii
Journal of applied chemistry of the USSR, 1987 , vol. 60, # 1 pt 2 p. 220 - 222
反应条件
in N,N-dimethyl-formamide T=100°C; 24 h;
参考文献
Inoue, Yoshio; Taguchi, Masaaki; Hashimoto, Harukichi
Synthesis, 1986 , # 4 p. 332 - 334
反应条件
sodium hydroxide; Methyl methyltrioctylammonium sulfate in toluene T=95°C; 4 h; different bases, other temperatures; Product distribution;
参考文献
Vasilevskaya; Grineva; Chernousova; Grankina; Andrievskii
Journal of applied chemistry of the USSR, 1987 , vol. 60, # 1 pt 2 p. 220 - 222
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C;
参考文献
Kowalski, Piotr; Mitka, Katarzyna; Jaskowska, Jolanta; Duszynska, Beata; Bojarski, Andrzej J.
Archiv der Pharmazie, 2013 , vol. 346, # 5 p. 339 - 348
反应条件
silver tetrafluoroborate; palladium diacetate in acetonitrile T=60°C;
参考文献
Desai, Lopa V.; Sanford, Melanie S.
Angewandte Chemie - International Edition, 2007 , vol. 46, # 30 p. 5737 - 5740
反应条件
sodium hydroxide in toluene T=80°C; 10 h;
参考文献
Ma, Chen; Zhang, Qian-Feng; Tan, Ye-Bang; Wang, Long
Journal of Chemical Research, 2004 , # 3 p. 186 - 187
