136918-14-4合成路线 （共 708 条）
反应条件
acetic acid 4.5 h; Reflux;
参考文献
Sajid, Muhammad; Jeschke, Gunnar; Wiebcke, Michael; Godt, Adelheid
Chemistry - A European Journal, 2009 , vol. 15, # 47 p. 12960 - 12962
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C; Alkylation; 8 h;
参考文献
Cho, Su-Dong; Kim, Hyeung-Jae; Ahn, Chuljin; Falckb; Shin, Dong-Soo
Tetrahedron Letters, 1999 , vol. 40, # 47 p. 8215 - 8217
反应条件
potassium fluoride on basic alumina in 2-methyl tetrahydrofuran T=83°C; 6 h; Inert atmosphere; chemoselective reaction;
参考文献
Pace, Vittorio; Hoyos, Pilar; Fernandez, Maria; Sinisterra, Jose V.; Alcantara, Andres R.
Green Chemistry, 2010 , vol. 12, # 8 p. 1380 - 1382
反应条件
1,4-diaza-bicyclo[2.2.2]octane; tetrabutyl-ammonium chloride in acetonitrile T=160°C; P=15001.2 Torr; 0.1 h;
参考文献
Shieh, Wen-Chung; Lozanov, Mario; Repic, Oljan
Tetrahedron Letters, 2003 , vol. 44, # 36 p. 6943 - 6945
反应条件
di-tert-butyl peroxide; copper diacetate in toluene T=100°C; 24 h; Sealed tubeInert atmosphere;
参考文献
Sueki, Shunsuke; Kuninobu, Yoichiro
Organic Letters, 2013 , vol. 15, # 7 p. 1544 - 1547
反应条件
2,6-bis(1,1-dimethylethyl)-p-benzoquinone in dichloromethane T=20°C; 1 h;
参考文献
Mukaiyama, Teruaki; Aoki, Hidenori
Chemistry Letters, 2005 , vol. 34, # 2 p. 142 - 143
反应条件
water; boric acid in 1,4-dioxane; toluene T=100°C; 4 h;
参考文献
Organic Letters, , vol. 14, # 12 p. 3202 - 3205
反应条件
in N,N-dimethyl-formamide
参考文献
Krafft, Grant A.; Siddall, Thomas L.
Tetrahedron Letters, 1985 , vol. 26, # 40 p. 4867 - 4870
反应条件
1: potassium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere 2: KHF2 / methanol; water; N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere 3: dichloro bis(acetonitrile) palladium(II); potassium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl / water; tert-butyl alcohol / 14 h / 100 °C / Inert atmosphere View Scheme
参考文献
Cul, Armelle; Daich, Adam; Decroix, Bernard; Sanz, Gerard; Van Hijfte, Luc
Heterocycles, 2004 , vol. 64, p. 33 - 39
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran -20 deg C to r.t.;
参考文献
Tetrahedron Letters, , vol. 33, # 25 p. 3607 - 3610
