136918-14-4合成路线 （共 708 条）
反应条件
1: HNO3+H2SO4 / Darstellung; Nitrierung 2: SnCl2; aqueous HCl 3: sodium nitrite; hydrochloric acid; water / 0 °C / Diazotization.beim Behandeln der erhaltenen Diazoniumsalz-Loesung mit Kupfer(I)-chlorid View Scheme
参考文献
Levy; Stephen
Journal of the Chemical Society, 1931 , p. 79,81
反应条件
1: caesium carbonate / acetonitrile / 80 °C 2: 0.5 h / Microwave irradiation View Scheme
参考文献
Long, Timothy E.; Lu, Xiao; Galizzi, Melina; Docampo, Roberto; Gut, Jiri; Rosenthal, Philip J.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 8 p. 2976 - 2979
反应条件
in benzene T=20°C; 144 h;
参考文献
Kukharev; Stankevich; Klimenko
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 10 p. 1434 - 1436
反应条件
1: 80 percent / 0.5 h / Heating 2: 63 percent / EDTA-Na2, Na2WO4*2HCl, aq. H2O2 / methanol / 72 h / 20 °C View Scheme
参考文献
Hankovszky; Hideg; Bodi; Frank
Journal of Medicinal Chemistry, 1986 , vol. 29, # 7 p. 1138 - 1152
反应条件
hydrogenchloride in water 10 h; Reflux;
参考文献
Gao, Weiming; Sun, Junliang; Akermark, Torbjoern; Li, Mingrun; Eriksson, Lars; Sun, Licheng; Akermark, Bjoern
Chemistry - A European Journal, 2010 , vol. 16, # 8 p. 2537 - 2546
反应条件
in acetonitrile 15 h; Irradiation;
参考文献
Journal of Organic Chemistry, , vol. 58, # 7 p. 1740 - 1745
反应条件
in acetonitrile 40 h; Irradiation;
参考文献
Journal of Organic Chemistry, , vol. 58, # 7 p. 1740 - 1745
反应条件
(i) Na, MeOH, (ii) Cl2, (iii) aq. HCl; Multistep reaction;
参考文献
Prout,F.S. et al.
Journal of Organic Chemistry, 1973 , vol. 38, p. 1512 - 1517
反应条件
palladium diacetate; oxygen in benzonitrile T=60°C; P=2660 Torr; 48 h;
参考文献
Brice, Jodie L.; Harang, Jenna E.; Timokhin, Vitaliy I.; Anastasi, Natia R.; Stahl, Shannon S.
Journal of the American Chemical Society, 2005 , vol. 127, # 9 p. 2868 - 2869
反应条件
oxygen; palladium diacetate in benzonitrile T=60°C; P=3040.2 Torr; 24 h; Title compound not separated from byproducts.;
参考文献
Rogers, Michelle M.; Kotov, Vasily; Chatwichien, Jaruwan; Stahl, Shannon S.
Organic Letters, 2007 , vol. 9, # 21 p. 4331 - 4334
