136918-14-4合成路线 (共 708 条)
反应条件
1: phthalimide With potassium hydroxide; Amberlite IRA-400 chloride form 2: 1,4-dibromo-butane in tetrahydrofuran Heating;
参考文献
Dalal; Pawar; Mahulikar
Organic Preparations and Procedures International, 2007 , vol. 39, # 1 p. 81 - 85
反应条件
potassium phtalimide Michael addition; 3 h; Inert atmosphereReflux;
参考文献
Dawadi, Prativa B. S.; Lugtenburg, Johan
European Journal of Organic Chemistry, 2008 , # 13 p. 2288 - 2292
参考文献
Passerini
Gazzetta Chimica Italiana, 1923 , vol. 53, p. 332
参考文献
Am. Cyanamid Co.
Patent: US2486210 , 1947 ;
反应条件
diethylazodicarboxylate in tetrahydrofuran 2 h;
参考文献
Grynkiewicz, Grzegorz
Polish Journal of Chemistry, 1982 , vol. 56, # 1 p. 149 - 152
反应条件
Mitsunobu conditions;
参考文献
Tiecco, Marcello; Testaferri, Lorenzo; Temperini, Andrea; Bagnoli, Luana; Marini, Francesca; Santi, Claudio; Terlizzi, Raffaella
European Journal of Organic Chemistry, 2004 , # 16 p. 3447 - 3458
反应条件
1: With pyridine; bromine in acetonitrile T=20°C; 2 h; 2: With methanol in acetonitrile 1 h; Cooling with ice;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 188, # 11 p. 1576 - 1583
反应条件
1: thiophenol With sulfuryl dichloride; triethylamine in dichloromethane T=0 - 20°C; 2: phthalimide With triethylamine in dichloromethane T=0 - 20°C; 1 h;
参考文献
Organic Letters, , vol. 16, # 3 p. 848 - 851
反应条件
triethylamine in diethyl ether
参考文献
Tetrahedron, , vol. 50, # 4 p. 1275 - 1294
反应条件
bromine in pyridine; acetonitrile 2 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 53, # 42 p. 14411 - 14416