136918-14-4合成路线 (共 708 条)
反应条件
triethylamine in dichloromethane T=0 - 20°C; 1 h;
参考文献
Gillis, H. Martin; Greene, Lana; Thompson, Alison
Synlett, 2009 , # 1 p. 112 - 116
反应条件
in N-methyl-acetamide
反应条件
triethylamine in hexane; N,N-dimethyl-formamide T=0 - 20°C; 1 h;
参考文献
Gillis, H. Martin; Greene, Lana; Thompson, Alison
Synlett, 2009 , # 1 p. 112 - 116
反应条件
1: ammonium hydroxide / 24 h 2: acetic anhydride / 2 h / |Reflux 3: 215 °C / 760.05 Torr / |Inert atmosphere View Scheme
参考文献
Engle, James T.; Allison, Ashley N.; Standard, Joshua M.; Tamgho, Ingrid-Suzy; Ziegler, Christopher J.
Journal of Porphyrins and Phthalocyanines, 2013 , vol. 17, # 8-9 p. 712 - 721
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran 0.25 h; Ambient temperature;
参考文献
Sammes, Peter G.; Thetford, Dean
Tetrahedron Letters, 1986 , vol. 27, # 20 p. 2275 - 2278
反应条件
[Pd(η3-1-Ph-allyl)(μ-Cl)]2; 1,3-bis-(diphenylphosphino)propane; sodium carbonate in toluene T=140°C; 20 h; Inert atmosphere; regioselective reaction;
参考文献
Banerjee, Debasis; Junge, Kathrin; Beller, Matthias
Angewandte Chemie - International Edition, 2014 , vol. 53, # 6 p. 1630 - 1635
Angew. Chem., 2014 , vol. 126, # 6 p. 1656 - 1661,6
反应条件
copper(l) chloride; benzene
参考文献
Fono
Chemistry and Industry (London, United Kingdom), 1958 , p. 414
反应条件
tert.-butylhydroperoxide; potassium iodide in water T=90°C; 1 h;
参考文献
Lao, Zhi-Qi; Zhong, Wen-He; Lou, Qing-Hua; Li, Zhong-Jun; Meng, Xiang-Bao
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 39 p. 7869 - 7871
参考文献
Coyle, John D.; Newport, Graham L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 93 - 96
反应条件
1: phthalimide With potassium carbonate in N,N-dimethyl-formamide 1 h; Reflux; 2: toluene-4-sulfonic acid 3-(1H-indol-3-yl)propyl ester in N,N-dimethyl-formamide Reflux;
参考文献
Archiv der Pharmazie, , vol. 347, # 3 p. 174 - 184