136918-14-4合成路线 （共 708 条）
反应条件
sodium methylate in dimethyl sulfoxide 2 h; Ambient temperature;
参考文献
Hammen; Braisted; Northrup
Synthetic Communications, 1991 , vol. 21, # 21 p. 2157 - 2163
反应条件
bis(η3-allyl-μ-chloropalladium(II)); S,S-DACHN; sodium carbonate optical yield given as percent ee;
参考文献
Llaveria, Josep; Diaz, Yolanda; Matheu, M. Isabel; Castillon, Sergio
European Journal of Organic Chemistry, 2011 , # 8 p. 1514 - 1519
反应条件
tetrabutyl-ammonium chloride; lithium carbonate; bis(η3-allyl-μ-chloropalladium(II)) in toluene T=40°C; Substitution; 40 h; Title compound not separated from byproducts;
参考文献
Harris, Michael C. J.; Jackson, Mark; Lennon, Ian C.; Ramsden, James A.; Samuel, Helen
Tetrahedron Letters, 2000 , vol. 41, # 17 p. 3187 - 3191
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; triethylamine; (S)-(+)-(3,5-dioxa-4-phosphacyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-bis-[(1S)-1-(2-methoxy-phenyl)ethyl]amine in tetrahydrofuran T=20°C; 24 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Gnamm, Christian; Franck, Geraldine; Miller, Nicole; Stork, Timon; Broedner, Kerstin; Helmchen, Guenter
Synthesis, 2008 , # 20 p. 3331 - 3350
反应条件
(R)-C4-TunePhos; sodium carbonate; [(ν3-allyl)PdCl]2 in tetrahydrofuran T=25°C; Product distribution; Further Variations:ReagentsSolventsTemperatures;
参考文献
Trost, Barry M.; Horne, Daniel B.; Woltering, Michael J.
Chemistry - A European Journal, 2006 , vol. 12, # 25 p. 6607 - 6620
反应条件
di-isopropyl azodicarboxylate; triphenylphosphine in tetrahydrofuran T=20°C; Mitsunobu reaction; 12 h;
参考文献
Dombi, Kendra L.; Griesang, Niels; Richert, Clemens
Synthesis, 2002 , # 6 p. 816 - 824
反应条件
1: potassium carbonate / 190 °C 2: sodium ethylate; ethanol 3: acetone; water; hydrogen peroxide View Scheme
参考文献
Schmid; Karrer
Helvetica Chimica Acta, 1948 , vol. 31, p. 1497,1500
反应条件
1: ammonium hydroxide / 24 h 2: acetic anhydride / 2 h / |Reflux View Scheme
参考文献
Engle, James T.; Allison, Ashley N.; Standard, Joshua M.; Tamgho, Ingrid-Suzy; Ziegler, Christopher J.
Journal of Porphyrins and Phthalocyanines, 2013 , vol. 17, # 8-9 p. 712 - 721
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C;
参考文献
Loska, Rafal; Janiga, Anita; Gryko, Dorota
Journal of Porphyrins and Phthalocyanines, 2013 , vol. 17, # 1-2 p. 104 - 117
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C;
参考文献
Kowalski, Piotr; Mitka, Katarzyna; Jaskowska, Jolanta; Duszynska, Beata; Bojarski, Andrzej J.
Archiv der Pharmazie, 2013 , vol. 346, # 5 p. 339 - 348
