136918-14-4合成路线 (共 708 条)
反应条件
potassium fluoride on basic alumina in 2-methyl tetrahydrofuran
T=90°C; 12 h; Inert atmosphere; chemoselective reaction;
参考文献
Pace, Vittorio; Hoyos, Pilar; Fernandez, Maria; Sinisterra, Jose V.; Alcantara, Andres R.
Green Chemistry, 2010 , vol. 12, # 8 p. 1380 - 1382
反应条件
copper(l) iodide; di-tert-butyl peroxide; 4,7-Dimethoxy-1,10-phenanthroline in benzene
T=100°C; 24 h; Inert atmosphere;
参考文献
Tran, Ba L.; Li, Bijie; Driess, Matthias; Hartwig, John F.
Journal of the American Chemical Society, 2014 , vol. 136, # 6 p. 2555 - 2563
反应条件
di-tert-butyl peroxide; (phthalimidato)copper(1,10-phenanthroline) in acetonitrile
T=100°C; 24 h; GloveboxInert atmosphere;
参考文献
Tran, Ba L.; Li, Bijie; Driess, Matthias; Hartwig, John F.
Journal of the American Chemical Society, 2014 , vol. 136, # 6 p. 2555 - 2563
反应条件
sodium hydroxide in water; acetonitrile
1.5 h; Irradiation;
参考文献
Suau, Rafael; Garcia-Segura, Rafael; Sanchez-Sanchez, Cristobal; Perez-Inestrosa, Ezequiel; Pedraza, Ana Maria
Tetrahedron, 2003 , vol. 59, # 16 p. 2913 - 2919
反应条件
sodium hydroxide in water; acetonitrile
Irradiation; Yields of byproduct given;
参考文献
Suau, Rafael; Garcia-Segura, Rafael; Sanchez, Cristobal; Pedraza, Ana Maria
Tetrahedron Letters, 1999 , vol. 40, # 10 p. 2007 - 2010
反应条件
sodium hydroxide in water; acetonitrile
T=20°C; 0.5 h; Irradiation; Further byproducts given;
参考文献
Suau, Rafael; Sanchez-Sanchez, Cristobal; Garcia-Segura, Rafael; Perez-Inestrosa, Ezequiel
European Journal of Organic Chemistry, 2002 , # 12 p. 1903 - 1911
反应条件
in N,N-dimethyl-formamide
Yield given;
参考文献
Krafft, Grant A.; Siddall, Thomas L.
Tetrahedron Letters, 1985 , vol. 26, # 40 p. 4867 - 4870
反应条件
water; boric acid in 1,4-dioxane; toluene
T=130°C; 24 h;
参考文献
Nguyen, Thanh Binh; Sorres, Jonathan; Tran, Minh Quan; Ermolenko, Ludmila; Al-Mourabit, Ali
Organic Letters, 2012 , vol. 14, # 12 p. 3202 - 3205
反应条件
pyridine; copper diacetate in dichloromethane
T=20°C;
参考文献
Huegel, Helmut M.; Rix, Colin J.; Fleck, Karin
Synlett, 2006 , # 14 p. 2290 - 2292
反应条件
copper diacetate; air in methanol
Heating;
参考文献
Lan, Jing-Bo; Zhang, Guo-Lin; Yu, Xiao-Qi; You, Jing-Song; Chen, Li; Yan, Mei; Xie, Ru-Gang
Synlett, 2004 , # 6 p. 1095 - 1097