136918-14-4合成路线 (共 708 条)
反应条件
copper
T=240°C; 12 h;
参考文献
Yamamoto, Takakazu; Kurata, Yasundo
Canadian Journal of Chemistry, 1983 , vol. 61, p. 86 - 91
反应条件
copper diacetate in dichloromethane; N,N-dimethyl-formamide
T=70°C; Arylation; 6 h;
参考文献
Lopez-Alvarado, Pilar; Avendano, Carmen; Menendez, J. Carlos
Journal of Organic Chemistry, 1996 , vol. 61, # 17 p. 5865 - 5870
反应条件
triethylamine; copper(I) bromide in dichloromethane
T=-40°C; 5 h; Inert atmosphere;
参考文献
Sueda, Takuya; Oshima, Ayumi; Teno, Naoki
Organic Letters, 2011 , vol. 13, # 15 p. 3996 - 3999
反应条件
[bis(acetoxy)iodo]benzene
T=140°C; 4 h; chemoselective reaction;
参考文献
Shrestha, Ruja; Mukherjee, Paramita; Tan, Yichen; Litman, Zachary C.; Hartwig, John F.
Journal of the American Chemical Society, 2013 , vol. 135, # 23 p. 8480 - 8483
反应条件
caesium carbonate in N,N-dimethyl-formamide
参考文献
Nuss, John M.; Harrison, Stephen D.; Ring, David B.; Boyce, Rustum S.; Johnson, Kirk; Pfister, Keith B.; Ramurthy, Savithri; Seely, Lynn; Wagman, Allan S.; Desai, Manjo; Levine, Barry H.
Patent: US2002/156087 A1, 2002 ;
US 20020156087 A1
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran
T=0 - 20°C; 22 h;
参考文献
Walker, Joel R; Curley Jr., Robert W
Tetrahedron, 2001 , vol. 57, # 31 p. 6695 - 6701
反应条件
sodium hydride
1) DMF, RT, 2.5h, 2) DMF, 24h; Yield given. Multistep reaction;
参考文献
Hitchings, Gregory J.; Helliwell, Madeleine; Vernon, John M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 1 p. 83 - 87
反应条件
potassium hydroxide; Aliquatreg; 336 in toluene
T=100°C; 4 h;
参考文献
Santaniello, Enzo; Ponti, Federico
Synthetic Communications, 1980 , vol. 10, # 8 p. 611 - 614
反应条件
potassium hydroxide; 1-n-butyl-3-methylimidazolium tetrafluoroborate
T=80°C; 4 h;
参考文献
Le, Zhang-Gao; Chen, Zhen-Chu; Hu, Yi; Zheng, Qin-Guo
Synthesis, 2004 , # 2 p. 208 - 212
参考文献
Roberts Laboratories Inc.
Patent: US6194420 B1, 2001 ;